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The Effect of Extrusion Parameters on the Microstructure and Mechanical Properties of TiCp/Mg-2.4Al-2.4Ca-0.6Mn Nanocomposites

  • Recent Advances in Multicomponent Alloys and Ceramics
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Abstract

TiCp/Mg-2.4Al-2.4Ca-0.6Mn (wt.%) nanocomposites have been extruded at different extrusion parameters. The grain of the composites was remarkably refined, and main second phase changed from the continuous network (Mg, Al)2Ca(C36) phase to the fractured (Mg, Al)2Ca(C36) phase with the decrease of extrusion temperature and speed. All the extruded composites displayed basal poles which are preferentially perpendicular to the extrusion direction (ED). As the extrusion speed increased, the basal plane (0002), prismatic type I side (10 \(\overline{1 }\) 0) and prismatic type II side (11 \(\overline{2 }\) 0) of TiCp/AXM2206 composites showed a weakening trend. The texture composition of extruded TiCp/AXM2206 composites was greatly affected by the degree of dynamic recrystallization (DRX) and the precipitates. The TiCp/Mg-Al-Ca-Mn nanocomposites exhibited excellent properties with tensile yield strength (TYS) of 400.3 MPa and ultimate strength (UTS) of 417.0 MPa. The improved strength was related to grain refinement, dislocation strengthening, thermal mismatch strengthening, and Orowan strengthening. During the tensile process, a large number of microcracks were formed along the (Mg, Al)2Ca(C36), resulting in structural failure.

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Acknowledgements

This work was supported by the National Natural Science Foundation of China [Grant Numbers 51771129, 51401144 and 51771128]; National Key Research and Development Program for Young Scientists [Grant. 2021YFB3703300]; the Program for the Outstanding Innovative Teams of Higher Learning Institutions of Shanxi; the Natural Science Foundation of Shanxi Province [Grant Numbers 2015021067 and 201601D011034]; and the Projects of International Cooperation in Shanxi [Grant No. 201703D421039]. Supported by Open Foundation of State Key Laboratory of Compressor Technology (Compressor Technology Laboratory of Anhui Province), No. SKL-YSJ202103.

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Authors and Affiliations

  1. College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, 030024, People’s Republic of China

    Hongwei Li, Kaibo Nie, An Yang & Kunkun Deng

  2. State Key Laboratory of Compressor Technology (Compressor Technology Laboratory of Anhui Province), Hefei, 230031, Anhui, People’s Republic of China

    Zhilong Liu

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Li, H., Nie, K., Liu, Z. et al. The Effect of Extrusion Parameters on the Microstructure and Mechanical Properties of TiCp/Mg-2.4Al-2.4Ca-0.6Mn Nanocomposites. JOM 74, 4226–4238 (2022). https://doi.org/10.1007/s11837-022-05475-x

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