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Effects of Sintering Temperature on Microstructure Evolution and Hot Deformation Behavior of TiAl-Based Alloys Prepared by Spark Plasma Sintering

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Abstract

TiAl-based alloys have been regarded as potential substitute materials for heavy Ni super-alloys. To understand the relationship of the processing-microstructure-hot deformation behavior of TiAl-based alloys fabricated via the spark plasma sintering technique, alloys were sintered at a temperature range of 1150–1350°C. Subsequently, isothermal compression tests were carried out at 1125°C with a strain rate of 0.1 s−1. The pre-alloyed powders, which showed dendritic structures, were mainly composed of α2 phase and a few of γ phase. Alloys composed of near gamma, duplex, and fully lamellar microstructures were obtained after sintering at 1150–1250°C, 1300°C, and 1350°C, respectively. The compressive peak stress increased with increasing sintering temperature, and the alloy sintered at 1250°C exhibited a better hot deformability. Moreover, dynamic recrystallization and phase transformation of α2 → γ occurred during isothermal compression.

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Acknowledgements

This work was supported by the Natural Science Foundation of China (Grant Nos. 51675125, 51675126) and the Natural Science Foundation of Heilongjiang Province (No. DC2013C048).

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Correspondence to Kaifeng Zhang or Zhen Lu.

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Shi, C., Han, M., Zhang, K. et al. Effects of Sintering Temperature on Microstructure Evolution and Hot Deformation Behavior of TiAl-Based Alloys Prepared by Spark Plasma Sintering. JOM 70, 2739–2745 (2018). https://doi.org/10.1007/s11837-018-3100-0

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  • DOI: https://doi.org/10.1007/s11837-018-3100-0

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