Skip to main content
Log in

Characterization of italian olive oils based on analytical and nuclear magnetic resonance determinations

  • Published:
Journal of the American Oil Chemists' Society

Abstract

Analytical measurements and proton nuclear magnetic resonance (1H NMR) spectra of phenolic extracts were performed on a set of italian extra-virgin olive oils from different cultivars and geographical locations of Apulia region. Multivariate statistical analysis (principal component analysis, hierarchical clustering analysis, and discriminant analysis) was applied separately to analytical and NMR data. Analytical parameters, in particular fatty acid compositions, permit the discrimination of olive variety, while 1H NMR data of phenolic extracts permit a classification according to the geographical origin of the samples.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Forina, M., and E. Tiscornia, Pattern Recognition Methods in the Prediction of Italian Olive Oil Origin by Their Fatty Acid Content, Ann. Chim. (Rome) 72:143–155 (1982).

    CAS  Google Scholar 

  2. Aparicio, R., L. Ferreiro, A. Cert, and A. Lanzon, Caraterización de aceites de oliva vírgenes andaluces, Grasas Aceites 41:23–39 (1990).

    CAS  Google Scholar 

  3. Tsimidou, M., and K.X. Karakostas, Geographical Classification of Greek Virgin Olive Oil by Nonparametric Multivariate Evaluation of Fatty Acid Composition, J. Sci. Food Agric. 62: 253–257 (1993).

    Article  CAS  Google Scholar 

  4. Sacchi, R., L. Mannina, P. Fiordiponti, P. Barone, L. Paolillo, M. Patumi, and A. Segre, Characterization of Italian Extra Virgin Olive Oils Using 1H NMR Spectroscopy, J. Agric. Food Chem. 46:3947–3951 (1998).

    Article  CAS  Google Scholar 

  5. Shaw, A.D., A. di Camillo, G. Vlahov, A. Jones, G. Bianchi, J. Rowland, and D.B. Kell, Discrimination of the Variety and Region of Origin of Extra Virgin Olive Oils Using 13C NMR and Multivariate Calibration with Variable Reduction, Anal. Chim. Acta 348:357–374 (1997).

    Article  CAS  Google Scholar 

  6. Spugnoli, P., A. Parenti, D. Cardini, G. Modi, and S. Caselli, Caratterizzazione di oli extra vergini monovarietali di tre cultivar toscane, Riv. Ital. Sostanze Grasse 75:227–233 (1998).

    CAS  Google Scholar 

  7. European Communities, Regulation 2568/91, Off. J. Eur. Communities, L 248 (1991).

    Google Scholar 

  8. Morrison, W.R., and L.H. Smith, Preparation of Fatty Acid Methyl Esters and Dimethylacetals from Lipids with Boron Fluoride-Methanol, J. Lipid Res. 64:373–376 (1964).

    Google Scholar 

  9. Massart, D.L., B.G.M. Vandeginste, S.N. Deming, Y. Michotte, and L. Kaufman, Chemometrics: A Textbook, Elsevier, New York, 1988, pp. 339–410.

    Google Scholar 

  10. Frank, I.E., and R. Todeschini, The Data Analysis Handbook, Elsevier Science B.V., Amsterdam, 1994, pp. 90, 153.

    Google Scholar 

  11. Solinas, M., L. Di Giovacchino, and A. Mascolo, The Polyphenols of Olives and Olive Oil. Note III: Influence of Temperature and Kneading Time on the Oil Polyphenol Content, Riv. Ital. Sostanze Grasse 55:19–23 (1978).

    CAS  Google Scholar 

  12. Solinas, M., HRGC Analysis of Phenolic Components in Virgin Olive Oil in Relation to the Ripening and the Variety of Olives, ——Ibid. 64:255–262 (1987).

    CAS  Google Scholar 

  13. Montedoro, G.F., and L. Garofolo, The Qualitative Characteristics of Virgin Olive Oils. The Influence of Variables Such as Variety, Environment, Preservation, Extraction, Conditioning of the Finished Product, ——Ibid. 61:157–168 (1984).

    CAS  Google Scholar 

  14. Amiot, M.T., A. Fleuriet, and J.T. Macheix, Importance and Evolution of Phenolic Compounds in Olive During Growth and Maturation, J. Agric. Food Chem. 34:823–826 (1986).

    Article  CAS  Google Scholar 

  15. Montedoro, G.F., M. Servili, M. Baldioli, R. Selvaggini, E. Miniati, and A. Macchioni, Simple and Hydrolyzable Compounds in Virgin Olive Oil. 3. Spectroscopic Characterization of the Secoiridoid Derivatives, ——Ibid. 41:2228–2234 (1993).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Antonio Sacco.

About this article

Cite this article

Sacco, A., Brescia, M.A., Liuzzi, V. et al. Characterization of italian olive oils based on analytical and nuclear magnetic resonance determinations. J Amer Oil Chem Soc 77, 619–625 (2000). https://doi.org/10.1007/s11746-000-0100-y

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11746-000-0100-y

Key Words

Navigation