Abstract
The most common environmental stress tests that are commonly used for corrosion risk assessment study or package integrity qualification qualifier as part of AEC-Q101E requirement are Unbiased highly accelerated stress test (u-HAST) and Unbiased humidity test(Moisture Soak). In this paper, this study is initiated due to abnormal situation whereby the failure could not be detected at 0 h as this corrosion symptom takes place after several months of storage (4 to 6 months) and failure can be only detected during customer board assembly process after subsequent period of storage. Objective of this paper is to develop a novel methodology by identifying an optimum environmental stress test condition which can replicate an early detection method to put in evidence the onset of corroded wedge on Cu-Ag system on a copper wire-bonded semiconductor device. The approach used was by subjecting the components to two different unbiased environmental stress methods, i.e., u-HAST and Moisture Soak. Pre- and post-electrical testing will be done after each interval for each stress tests. In the event if there are no electrical failures observed, post-mechanical decapsulation analysis results will be used instead. Upon mechanical decapsulation, the visual inspection on the wedge surface area and periphery of Ag plating was performed through optical inspection. x-ray Photoelectron Spectroscopy (XPS) will complement the Energy Dispersive x-ray (EDX) analysis to confirm the corrosion product on the wedge surface area and periphery of Ag plating area surrounding the wedge surface. Based on the evaluation results, Moisture Soak, clearly demonstrated a better leading indicator compared to u-HAST for the activation of corrosion. Moisture Soak (55 °C/85%RH) showing a consistent trend of higher corrosion detection on SOT23 package compared to u-HAST.
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References
G. Harman, Wirebonding in microelectronics, materials, processes, reliability and yield, 3 (Edn) (McGraw-Hill Professional, New York, 1997), p. 19–97
W. Wang, A. Choubey, M.H. Azarian, M. Pecht, An assessment of immersion silver surface finish for lead free electronics. J. Elect. Mater. 38, 815–827 (2009). https://doi.org/10.1007/s11664-009-0761-z
T.K. Lee, C.D. Breach, W.L. Chong, C.S. Goh Oxidation and corrosion of Au/Al and Cu/Al in wire bonding assembly. In: 2012 13th International Conference on Electronic Packaging Technology & High Density Packaging. pp. 244–249 (2012). doi: https://doi.org/10.1109/ICEPT-HDP.2012.6474610.
C.-U. Kim and J.-Y. Chang Corrosion in a closed-loop electronic device cooling system with water as coolant and its detection. In: 2017 16th IEEE Intersociety Conference on Thermal and Thermomechanical Phenomena in Electronic Systems (ITherm). pp. 558–564 (2017). doi: https://doi.org/10.1109/ITHERM.2017.7992536.
Hualiang Huang, Bu. Furong, Correlations between the inhibition performances and the inhibitor structures of some azoles on the galvanic corrosion of copper coupled with silver in artificial seawater. Corros. Sci. 165, 108413 (2019). https://doi.org/10.1016/j.corsci.2019.108413
D. Lee, J. Lee, C.C. Chen, A. Lin, Evaluation of the Anti-Corrosion Capacity for Various Electronics by Way of Accelerated Corrosion Testing Platform. Inst Microelect. Packag. Assem. Cir. Technol. Conf. (2021). https://doi.org/10.1109/IMPACT.2016.7800066
B. Christopher, N.H. Shen, Teck Kheng Lee, R.J. Holliday, Corrosion of gold and copper ball bonds. ECS Trans. 34(1): 831–841 (2011)
T. Uno, T. Yamada, Improving humidity bond reliability of copper bonding wires. In: 2010 Proceedings 60th electronic components and technology conference (ECTC). pp 1725–1732 (2010). doi: https://doi.org/10.1109/ECTC.2010.5490741.
J.Y. Glacet, G. Guerri Dall’oro, Low-cost physical analysis techniques for the failure analysis of semiconductor components. Qual. Reliab. Eng. Int. 8(2), 93–98 (2007). https://doi.org/10.1002/qre.4680080204E
J.M. Cano, J.L. Bastidas, N. Polo, Mora, study of the effect of acetic acid vapor on copper corrosion at 40 and 80% relative humidity. J. Electrochem. Soc. 148, B431–B437 (2001)
D.W. Rice, P. Peterson, E.B. Rigby, P.B.P. Phipps, R.J. Cappell, R. Tremoureux, Atmospheric corrosion of copper and silver. J. Electrochem. Soc. 128, 275–284 (1981)
F. Samie, J. Tidblad, V. Kucera, C. Leygraf, Atmospheric corrosion effects of HNO3 -Influence of temperature and relative humidity on labaoratory exposed copper. Atmos. Environ. 41, 1374–1382 (2007). https://doi.org/10.1016/j.atmosenv.2006.10.018
P. Eriksson, L.G. Johansson, H. Strandberg, Initial stages of copper corrosion in humid air containing SO2 and NO2. J. Electrochem. Soc. 140, 53–59 (1993)
W.H.J. Vernon, Trans A laboratory study of the atmospheric corrosion of metals Part 1-The corrosion of copper in certain synthethic atmospeheres wuth particular reference to the infleunce of sulfur dioxide in air of various relative humidities. Faraday Soc. 27: 255–277 (1931)
Annika Niklasson, Lars-Gunnar Johansson, Jan-Erik Svensson. The infleunce of relative humidity and temperature on the acetic acid vapour-induced atmospheric corrosion of lead. Corros. Sci. 50(11): 303–307 (2008). doi https://doi.org/10.1016/j.corsci.2008.08.009
Nurul Syafiqah Mohd Azmi, Danial Mohamed, Mohd Yuhyi Mohd Tadza, Effects of various relative humidity conditions on copper corrosion behavior in bentonite. Materials Today: Proceedings 2022 Elsevier. (2022)
C.-P. Liu et al. Corrosion-induced degradation and its mechanism study of Cu–Al interface for Cu-wire bonding under HAST conditions. J. Alloys Comp. 825: 154046 (2020). doi https://doi.org/10.1016/j.jallcom.2020.154046
K. Abhishek, D. Samet, V.N.N. Trilochan Rambhatla, S.K. Sitaraman (2020) Effect of temperature and humidity conditioning on copper leadframe/mold compound interfacial delamination. Microelect. Reliab. 111: 113647. doi https://doi.org/10.1016/j.microrel.2020.113647
D. Udiljak, R. Pufall, G. M. Reuther, J. Boudaden, P. Ramm, G. Schrag. Humidity and corrosion susceptibility of molded packages under mechanical impact Novel package level impact test to provoke micro-damage. In: 2022 23rd International Conference on Thermal, Mechanical and Multi-Physics Simulation and Experiments in Microelectronics and Microsystems (EuroSimE), pp. 1–8 (2022). doi: https://doi.org/10.1109/EuroSimE54907.2022.9758867.
K. Hamid, K. A, A. H, Badarisman, A. Jalar, M.A. Bakar. Investigation of integrated factors in the occurrence of copper wire bonding corrosion of semiconductor packages. J. Phys. Conf. Ser. 2169(1): 012016 (2022). doi:https://doi.org/10.1088/1742-6596/2169/1/012016
A.J. Garete, Z. Li, A. Taduran, M.N.A. Balasundaram, Enabling MSL1 Zero Delamination through Advanced Packaging Solutions for Robust Automotive Power Package. In: 15th IMPACT, Taipei, Taiwan. pp. 99–102 (2020). doi: https://doi.org/10.1109/IMPACT50485.2020.9268544.
T. Li, A. He, P. Chen, L. Ng, H. Yuan, PMC Effect Study on Package Delamination with Different EMC type. In: 21st ICEPT, Guangzhou, China. pp. 1–4 (2020) doi: https://doi.org/10.1109/ICEPT50128.2020.9202991.
Acknowledgment
The authors would like to express our appreciation to the Reliability Laboratory team, Material Analysis Team who have support us with the analysis for this project. The authors would like to acknowledge the financial support and research facilities provided by the Ministry of Higher Education, Malaysia under Fundamental Research Grant Scheme (FRGS/1/2020/TK0/UKM/01/3).
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Supramaniam, S., Bakar, M.A. & Jalar, A. Early Corrosion Detection of Cu-Ag Wedge bonding in Semiconductor Package. J Fail. Anal. and Preven. 22, 2317–2325 (2022). https://doi.org/10.1007/s11668-022-01528-0
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DOI: https://doi.org/10.1007/s11668-022-01528-0