Abstract
SiCp/Mg composites, where a minor amount of SiCp was added to the pure Mg, were fabricated in this work to eliminate the influence of precipitates and determine the effect of the particle deformation zone on the microstructure, texture and mechanical properties of the Mg matrix. The results show that the dynamically recrystallized ratio in the SiCp/Mg composite obviously improved because SiCp promoted the nucleation of DRX. Compared with those of the pure Mg, the SiCp/Mg composite had finer grain sizes and weaker basal textures. Even when only 1 vol.% SiCp was added to the pure Mg, the yield strength, ultimate tensile strength and elongation of pure Mg could be increased to 247.3 MPa, 260.36 MPa and 6.85%, respectively. Such high strength of the SiCp/Mg composite might attribute to the fine grain size as well as nano-MgO precipitates after the addition of a minor amount of SiCp.
Similar content being viewed by others
References
Q.X. Shi, C.J. Wang, K.K. Deng, K.B. Nie, M. Cao, W.M. Gan, and W. Liang, Work hardening and softening behavior of pure Mg influenced by Zn addition investigated via in-situ neutron diffraction, Mater. Sci. Eng. A, 2020, 772, p 138827
R.K. Mishra, A.K. Gupta, P.R. Rao, A.K. Sachdev, A.M. Kumar, and A.A. Luo, Influence of Cerium on the Texture and Ductility of Magnesium Extrusions, Scrip. Mater., 2008, 59(5), p 562–565
A. Yamashita, Z. Horita, and T.G. Langdon, Improving the Mechanical Properties of Magnesium and a Magnesium Alloy Through Severe Plastic Deformation, Mater. Sci. Eng. A, 2001, 300(1), p 142–147
R.A. Saravanan and M.K. Surappa, Fabrication and Characterisation of Pure Magnesium-30 vol.% SiCP Particle Composite, Mater. Sci. Eng. A, 2000, 276(1), p 108–116
X.J. Wang, H.U. Xiao-Shi, K.B. Nie, W.U. Kun, and M.Y. Zheng, Hot Extrusion of SiCp/AZ91 Mg Matrix Composites, Trans. Nonferr. Metals Soc. China, 2012, 22(8), p 1912–1917
X.J. Wang, N.Z. Wang, L.Y. Wang, X.S. Hu, K. Wu, Y.Q. Wang, and Y.D. Huang, Processing, Microstructure and Mechanical Properties of Micro-SiC Particles Reinforced Magnesium Matrix Composites Fabricated by Stir Casting Assisted by Ultrasonic Treatment Processing, Mater. Des., 2014, 57, p 638–645
R.D. Doherty, D.A. Hughes, F.J. Humphreys, J.J. Jonas, D.J. Jensen, M.E. Kassner, W.E. King, T.R. Mcnelley, H.J. Mcqueen, and A.D. Rollett, Current Issues in Recrystallization: A Review, Mater. Sci. Eng. A, 1997, 238(2), p 219–274
X.J. Wang, X.S. Hu, W.Q. Liu, J.F. Du, K. Wu, Y.D. Huang, and M.Y. Zheng, Ageing Behavior of as-Cast SiCp/AZ91 Mg Matrix Composites, Mater. Sci. Eng. A, 2017, 682, p 491–500
X.F. Sun, C.J. Wang, K.K. Deng, J.W. Kang, Y. Bai, K.B. Nie, and S.J. Shang, Aging Behavior of AZ91 Matrix Influenced by 5 μm SiCp: Investigation on the Microstructure and Mechanical Properties, J. Alloys Compd., 2017, 727, p 1263–1272
W.J. Li, K.K. Deng, X. Zhang, C.J. Wang, J.W. Kang, K.B. Nie, and W. Liang, Microstructures, Tensile Properties and Work Hardening Behavior of SiCp/Mg-Zn-Ca Composites, J. Alloys Compd., 2017, 695, p 2215–2223
L.B. Tong, M.Y. Zheng, L.R. Cheng, S. Kamado, and H.J. Zhang, Effect of Extrusion Ratio on Microstructure, Texture and Mechanical Properties of Indirectly Extruded Mg-Zn-Ca Alloy, Mater. Sci. Eng. A, 2013, 569, p 48–53
A. Imandoust, C.D. Barrett, A.L. Oppedal, W.R. Whittington, and H.E. Kadiri, Nucleation and Preferential Growth Mechanism of Recrystallization Texture in High Purity Binary Magnesium-Rare Earth Alloys, Acta Mater., 2017, 138, p 27–41
W. Tang, S. Huang, S. Zhang, D. Li, and Y. Peng, Influence of Extrusion Parameters on Grain Size and Texture Distributions of AZ31 Alloy, J. Mater. Process. Technol., 2011, 211(7), p 1203–1209
Y.Z. Du, M.Y. Zheng, C. Xu, X.G. Qiao, K. Wu, X.D. Liu, G.J. Wang, and X.Y. Lv, Microstructures and Mechanical Properties of as-Cast and as-Extruded Mg-4.50Zn-1.13Ca (wt%) Alloys, Mater. Sci. Eng. A, 2013, 576(6), p 6–13
W.M. Gan, M.Y. Zheng, H. Chang, X.J. Wang, X.G. Qiao, K. Wu, B. Schwebke, and H.G. Brokmeier, Microstructure and Tensile Property of the ECAPed Pure Magnesium, J. Alloys Compd., 2009, 470(1), p 256–262
Q. Li and T. Bing, Mechanical Properties and Microstructure of Pure Polycrystalline Magnesium Rolled by Different Routes, Mat. Lett., 2012, 67(1), p 81–83
M. Shanthi, P. Jayaramanavar, V. Vyas, D.V.S. Seenivasan, and M. Gupta, Effect of Niobium Particulate Addition on the Microstructure and Mechanical Properties of Pure Magnesium, J. Alloys Compd., 2012, 513(4), p 202–207
H.F. Sun, L.I. Cheng-Jie, Y. Xie, and W.B. Fang, Microstructures and Mechanical Properties of Pure Magnesium Bars by High Ratio Extrusion and Its Subsequent Annealing Treatment, Trans. Nonferr. Metal. Soc. China, 2012, 22(12), p s445–s449
P. Pérez, G. Garcés, and P. Adeva, Influence of Texture on the Mechanical Properties of Commercially Pure Magnesium Prepared by Powder Metallurgy, J. Mater. Sci., 2007, 42(11), p 3969–3976
C.S. Goh, J. Wei, L.C. Lee, and M. Gupta, Properties and Deformation Behaviour of Mg-Y2O3 Nanocomposites, Acta Mater., 2007, 55(15), p 5115–5121
G.S. Rao and Y.V.R.K. Prasad, Grain Boundary Strengthening in Strongly Textured Magnesium Produced by Hot Rolling, Metall. Trans. A, 1982, 13(12), p 2219–2226
W.L. Cheng, Q.W. Tian, H. Yu, H. Zhang, and B.S. You, Strengthening Mechanisms of Indirect-Extruded Mg-Sn Based Alloys at Room Temperature, J. Mag. Alloys, 2014, 2(4), p 299–304
K.B. Nie, X.J. Wang, F.J. Xu, K. Wu, and M.Y. Zheng, Microstructure and Tensile Properties of SiC Nanoparticles Reinforced Magnesium Matrix Composite Prepared by Multidirectional Forging Under Decreasing Temperature Conditions, Mater. Sci. Eng. A, 2015, 639, p 465–473
Q.B. Nguyen and M. Gupta, Enhancing Compressive Response of AZ31B Magnesium Alloy Using Alumina Nanoparticulates, Compos. Sci. Technol., 2008, 68(10–11), p 2185–2192
Acknowledgments
This work was supported by “National Natural Science Foundation of China” (Grants 51771128 and 51771129), Projects of International Cooperation in Shanxi (Grant No. 201703D421039), Shanxi Province Science and Technology Major Projects (Grant No. 20181101008) and the Program for the Outstanding Innovative Teams of Higher Learning Institutions of Shanxi.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Shi, Qx., Deng, Kk., Nie, Kb. et al. Significant Influence of Minor SiCp on Microstructure and Mechanical Properties of Pure Mg. J. of Materi Eng and Perform 29, 1356–1365 (2020). https://doi.org/10.1007/s11665-020-04627-x
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-020-04627-x