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Analysis of Splitting and Martensitic Transformation of AlNi Intermetallic Obtained by Transient Liquid Phase Bonding

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Abstract

This study investigates the characteristics of the AlNi intermetallic formed in a Ni/Al/Ni couple obtained by the Transient Liquid Phase Bonding (TLPB) process. The crystal structure and orientation of the AlNi intermetallic phase were evaluated through SEM-EDS EBSD and its mechanical properties were analyzed by means of instrumented hardness. The results showed that AlNi intermetallic splits into two layers, with different Al content and the same crystal structure and orientation. EBSD mapping revealed that there is no grain boundary along the split line, suggesting that a chemical partition takes place without the need of nucleation, like in a spinodal decomposition. A martensitic layer formed at the Ni-rich AlNi split side was identified by indexing the measured Kikuchi patterns. Instrumented hardness showed that the mechanical properties of AlNi phase change markedly depending on its chemical composition. These results provide experimental data that contribute to the understanding of the solid-state transformations occurring in the central portion of the Al-Ni phase diagram under isothermal conditions.

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Acknowledgments

Authors wish to express their gratitude to CONICET (Consejo Nacional de Investigaciones Científicas y Técnicas) and to Christian Doppler Forschungsgesellschaft, fostered in the frame of CD-Laboratory for Design of High-Performance Alloys by Thermomechanical Processing, for their financial support.

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Authors and Affiliations

  1. Materials Characterization, IITCI CONICET-UNCo, Buenos Aires 1400, 8300, Neuquén, Argentina

    Mariana Poliserpi & Silvana Sommadossi

  2. Metallurgy Division, INTEMA CONICET-UNMdP, Av. Juan B. Justo 4302, B7608FDQ, Mar del Plata, Argentina

    Roberto Boeri

  3. Institute of Materials Science, Joining and Forming, TU-Graz, Kopernikusgasse 24/I, 8010, Graz, Austria

    Ricardo Buzolin & Cecilia Poletti

  4. Christian Doppler Laboratory for Design of High-Performance Alloys by Thermomechanical Processing, Kopernikusgasse 24/I, 8010, Graz, Austria

    Ricardo Buzolin & Cecilia Poletti

Authors
  1. Mariana Poliserpi
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  2. Ricardo Buzolin
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  3. Roberto Boeri
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  4. Cecilia Poletti
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  5. Silvana Sommadossi
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Correspondence to Mariana Poliserpi.

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Manuscript submitted September 19, 2019.

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Poliserpi, M., Buzolin, R., Boeri, R. et al. Analysis of Splitting and Martensitic Transformation of AlNi Intermetallic Obtained by Transient Liquid Phase Bonding. Metall Mater Trans B 51, 916–924 (2020). https://doi.org/10.1007/s11663-020-01832-w

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  • DOI: https://doi.org/10.1007/s11663-020-01832-w

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