Abstract
Using a variety of depth-sensing indentation techniques, the creep response of high-purity indium, from room temperature to 75 °C, was measured. The dependence of the hardness on the variables of indentation strain rate (stress exponent for creep (n)) and temperature (apparent activation energy for creep (Q)) and the existence of a steady-state behavior in an indentation test with a Berkovich indenter were investigated. It was shown for the first time that the indentation strain rate (-este-/h) could be held constant during an experiment using a Berkovich indenter, by maintaining the loading rate divided by the load (-este-/P) constant. The apparent activation energy for indentation creep was found to be 78 kJ/mol, in accord with the activation energy for self-diffusion in the material. Finally, by performing -este-/P change experiments, it was shown that a steady-state path independent of hardness could be reached in an indentation test with a geometrically similar indenter.
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A.G. Atkins, A. Silverio, and D. Tabor: J. Inst. Met., 1966, vol. 94, pp. 369–78.
S. Hannula, D.S. Stone, and C.Y. Li: Electronic Packaging Materials Science, Materials Research Society Symposia Proceedings, E.A. Geiss, K.N. Tu, and D.R. Uhlmann, eds., Materials Research Society, Pittsburgh, PA, 1985, vol. 40, pp. 217–24.
W.R. LaFontaine, B. Yost, R.D. Black, and C.-Y. Li: J. Mater. Res., 1990, vol. 5, pp. 2100–06.
M.J. Mayo and W.D. Nix: Acta Metall., 1988, vol. 36, pp. 2183–92.
M.J. Mayo and W.D. Nix: in Strength of Metals and Alloys, P.O. Kettunen, T.K. Lepisto, and M.E. Lehtonen, eds., Pergamon Press, Elms ford, NY, 1988, pp. 1415–20.
H.M. Pollock, D. Maugis, and M. Barquins: in Microindentation Techniques in Materials Science and Engineering, P.J. Blau and B.R. Lawn, eds., ASTM, Philadelphia, PA, 1986, pp. 47–71.
M.J. Mayo, R.W. Siegel, Y.X. Liao, and W.D. Nix: J. Mater. Res., 1992, vol. 7, pp. 973–79.
M.J. Mayo, R.W. Siegel, A. Narayanasamy, and W.D. Nix: J. Mater. Res., 1990, vol. 5, pp. 1073–82.
V. Raman and R. Berriche: Thin Films: Stresses and Mechanical Properties II, Materials Research Society Symposia Proceedings, M.F. Doerner, W.C. Oliver, G.M. Pharr, and F.R. Brotzen, eds., Materials Research Society, Pittsburgh, PA, 1990, vol. 188, pp. 171–76.
V. Raman and R. Berriche: J. Mater. Res., 1992, vol. 7, pp. 627–38.
B.N. Lucas and W.C. Oliver: Thin Films: Stresses and Mechanical Properties III, Materials Research Society Symposia Proceedings, W.D. Nix, J.C. Bravman, E. Arzt, and L.B. Freund, eds., Materials Research Society, Pittsburgh, PA, 1992, vol. 239, pp. 337–41.
S.N.G. Chu and J.C.M. Li: J. Mater. Sci., 1977, vol. 12, pp. 2200–08.
S.N.G. Chu and J.C.M. Li: Mater. Sci. Eng., 1979, vol. 39, pp. 1–10.
W.H. Poisl, W.C. Oliver, and B.D. Fabes: J. Mater. Res., 1995, vol. 10, pp. 2024–32.
S.P. Baker, J.T.W. Barbee, and W.D. Nix: Thin Films: Stresses and Mechanical Properties III, Materials Research Society Symposia Proceedings, W.D. Nix, J.C. Bravman, E. Arzt, and L.B. Freund, eds., Materials Research Society, Pittsburgh, PA, 1992, vol. 239, pp. 337–41.
K.B. Yoder, D.S. Stone, J.C. Lin, and R.A. Hoffman: Thin Films: Stresses and Mechanical Properties V, Materials Research Society Symposia Proceedings, S.P. Baker, C.A. Ross, P.H. Townsend, C.A. Volkert, and P. Borgesen, eds., Materials Research Society, 1994, vol. 356, pp. 651–56.
E.C. Yu and J.C.M. Li: Phil. Mag., 1977, vol. 36, pp. 811–25.
D.S. Stone and K.B. Yoder: J. Mater. Res., 1994, vol. 9, pp. 2524–33.
M.F. Doerner and W.D. Nix: J. Mater. Res., 1986, vol. 1, pp. 601–09.
B.N. Lucas: Ph.D. Dissertation, The University of Tennessee, Knoxville, TN, 1997.
J. Weertman: Trans. AIME, 1960, vol. 218, pp. 207–18.
N.A. Stilwell and D. Tabor: Proc. Phys. Soc. London, 1961, vol. 78, pp. 169–79.
R.E. Eckert and H.G. Drickamer: J. Chem. Phys., 1952, vol. 20, pp. 13–17.
G.W. Powell and J.D. Braun: Trans. AIME, 1960, vol. 230, pp. 694–99.
O.D. Sherby and A.K. Miller: ASME J. Mater. Technol., 1979, vol. 101, pp. 387–95.
O.D. Sherby: Acta Metall., 1962, vol. 10, pp. 135–47.
C.R. Barrett, A.J. Ardell, and O.D. Sherby: Trans. TMS-AIME, 1964, vol. 230, pp. 200–04.
J. Weertman, W.V. Green, and E.G. Zukas: J. Mater. Sci. Eng., 1970, vol. 6, pp. 199–211.
D.S. Tabor: Proc. R. Soc. A, 1948, vol. 192, pp. 247–74.
K.L. Johnson: J. Mech. Phys. Solids, 1970, vol. 18, pp. 115–26.
S.S. Chiang, D.B. Marshall, and A.G. Evans: J. Appl. Phys., 1982, vol. 53, pp. 298–311.
A.F. Bower, N.A. Fleck, A. Needleman, and N. Ogbonna: Proc. R. Soc. London A, 1993, vol. 441, pp. 97–124.
D.S. Tabor: Hardness of Metals, Clarendon Press, Oxford, United Kingdom, 1951, pp. 103–07.
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Lucas, B.N., Oliver, W.C. Indentation power-law creep of high-purity indium. Metall Mater Trans A 30, 601–610 (1999). https://doi.org/10.1007/s11661-999-0051-7
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DOI: https://doi.org/10.1007/s11661-999-0051-7