Abstract
Micro compression and micro extrusion experiments of ultrafine grained titanium cylindrical specimens in diameters of 4, 2, and 1 mm prepared by equal channel angular pressing (ECAP) were conducted on the micro plastic forming test machine. The effects of specimen size, grain size, deformation temperature and extrusion speed on the flow stress and forming properties of the ultrafine grained pure titanium were investigated. The flow stress of ultrafine grained pure titanium specimen decreases with decreasing specimen size. The yield limit of pure titanium with refined grain prepared by ECAP is significantly greater than that of coarse grained specimen. Also the research results show that the flow stress of specimen increases with decreasing deformation temperature and with the increase of the strain rate, and the ultrafine grained pure titanium possesses good micro forming properties at deformation temperature of 300 °C.
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Geiger M, Kleiner M, Tiesler R, et al. Microforming[J]. Annals of the CIRP, 2001, 50(2): 445–462
Geiger M, Merklein M and Tolazzi M. Metal Forming Ensures Innovation and Future in Europe[C]. In: Proceedings of the 8th International Conference on Technology of Plasticity, Verona, 2005: 25–30
Engel U and Eckstein R. Microforming-from Basic Research to Its Realization[J]. Journal of Materials Processing Technology, 2002, 125–126:35–44
Vollertsen F, Niehoff HS and Hu Z. State of the Art in Micro Forming[J]. International Journal of Machine Tools & Manufacture, 2006, 46(11): 1172–1179
Latysh V, Krallics G, Alexandrov IV, et al. Application of Bulk Nanostructured Materials in Medicine[J]. Current Applied Physics, 2006, 6(2): 262–266
Zhernakov VS, Latysh VV, Stolyarov VV, et al. The Developing of Nanostructured SPD Ti for Structural Use[J]. Scripta Materialia, 2001, 44(8): 1771–1774
Dalla Torre FH, Lapovok RY, Sandlin JD, et al. Microstructures and Properties of Copper Proce-ssed by Equal Channel Angular Extrusion for 1–16 Passes[J]. Acta Materialia, 2004, 52(16): 4819–4832
Valiev RZ, Islamgaliev RK and Alexandrov IV. Bulk Nano-structured Materials from Severe Plastic Deformation[J]. Progress in Materials Science, 2000, 45: 103–189
Neishi K, Hotita TG. Archieving Superplasti-city in Ulterfine-grained Copper: Influence of Zn and Zr Additions[J]. Materials Science and Engineering, 2003, A352(1–2): 129–135
Wang GC, Zheng W, Jiang H, et al. Experimental Research on Size Effect of Micro Upsetting of Pure Copper[J]. Journal of Mechanical Engineering, 2012, 48(14): 32–37
Guo B, Gong F, Wang CJ, et al. Flow Stress and Tribology Size Effects in Scaled Down Cylinder Compression[J]. Trans.Nonferrous Met. Soc., 2009, 19(s2): s516–s520
Chen FK and Tsai JW. A Study of Size Effect in Micro-forming with Micro-hardness Tests[J]. Journal of Materials Processing Technology, 2006, 177(1): 146–149
Zhu XF. Ultrafine-grained Aluminum Micro Compression Deformation Behavior and Microstru-cture Evolution[D]. Harbin: Harbin Institute of Technology, 2013
Zhou ML. The Similarity of Sciences[M]. Beijing: Science Press, 2004
Dong XH, Wang Q, Zhang HM, et al. Research Progress of Size Effect of Micro Forming[J]. Scientia Sinica Techologica, 2013, 43(2): 115–130
Trelewicz J, Schuh C. The Hall-Petch Breakdown in Nanocrystalline Metals: A Crossover to Glass-like Deformation[J]. Acta Materialia, 2007, 55(17): 5948–5958
Aifantis KE, Konstantinidis AA. Hall-Petch Revisited at the Nanoscale[J]. Materials Science & Engineering B, 2009, 163(3): 139–144
Geiger M, Kleinera M, Eckstein R, et al. Microforming[J]. CIRP Annals-Manufacturing Technology, 2001, 50(2): 445–462
Guo B, Gong F and Shan D. Research Progress of Tribology in Microforming[J]. Journal of Plasticity Engineering, 2009, 16(4): 146–151
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Funded by the National Natural Science Foundation of China ( No. 51474170) and the SAN JIN Scholars Program
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Wang, X., Liu, J., Zhao, X. et al. Micro extrusion of ultrafine grained titanium prepared by ECAP. J. Wuhan Univ. Technol.-Mat. Sci. Edit. 32, 437–443 (2017). https://doi.org/10.1007/s11595-017-1616-8
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DOI: https://doi.org/10.1007/s11595-017-1616-8