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Analyses of nitrobenzene, benzene and aniline in environmental water samples by headspace solid phase microextraction coupled with gas chromatography-mass spectrometry

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Chinese Science Bulletin

Abstract

A headspace solid phase microextraction coupled with gas chromatography mass spectrometry (HS-SPME/GC-MS) method was established for analyzing nitrobenzene, benzene and aniline in environmental water samples simultaneously. Factors affecting extraction efficiency (SPME fiber selection, acidity, temperature, salt addition, extraction time, headspace, etc) were verified. Under optimal extraction conditions, the detection limits are 0.50, 0.11 and 1.00 μg/L for nitrobenzene, benzene and aniline, respectively. The results indicate that this method is capable of making sensitive and accuracy analyses on nitrobenzene, benzene and aniline in environmental water samples.

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Authors and Affiliations

  1. State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-environmental Sciences, Chinese Academy of Sciences, Beijing, 100085, China

    Chen Ming, Yin Yongguang, Tai Chao, Zhang Qinghua, Liu Jiyan & Jiang Guibin

  2. School of Chemistry and Chemical Engineering, Shandong University, Ji’nan, 250100, China

    Chen Ming & Hu Jingtian

Authors
  1. Chen Ming
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  2. Yin Yongguang
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  3. Tai Chao
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  4. Zhang Qinghua
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  5. Liu Jiyan
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  6. Hu Jingtian
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  7. Jiang Guibin
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Corresponding author

Correspondence to Jiang Guibin.

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Chen, M., Yin, Y., Tai, C. et al. Analyses of nitrobenzene, benzene and aniline in environmental water samples by headspace solid phase microextraction coupled with gas chromatography-mass spectrometry. CHINESE SCI BULL 51, 1648–1651 (2006). https://doi.org/10.1007/s11434-006-2020-5

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  • DOI: https://doi.org/10.1007/s11434-006-2020-5

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