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Titanium-monosubstituted polyoxometalates: relation between homogeneous and heterogeneous Ti-single-site-based catalysis

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The similarity in the catalytic behaviour of titanium-monosubstituted Keggin type polyoxometalates [PTi(L)W11O39]n- (Ti-POMs) and heterogeneous titanium single-site catalysts in selective oxidations with H2O2 is demonstrated. Recent achievements in the application of Ti-POMs as soluble molecular models for studying mechanisms of oxidation catalysis are reviewed.

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Abbreviations

BPS:

benzyl phenyl sulfide

BP:

2,2´,3,3´,5,5´-hexamethyl-4,4´-biphenol

CyH:

cyclohexene

MPS:

methyl phenyl sulphide

MPSO:

methyl phenyl sulfoxide

MPSO2 :

methyl phenyl sulfone

POM:

polyoxometalate

TMP:

2,3,6-trimethylphenol

TMBQ:

2,3,5-trimethyl-1,4-benzoquinone

TBA:

tetra-n-butylammonium

Ti-POM or PW11TiL:

[PTi(L)W11O39]n-

(PW11Ti)2OH:

[Bu4N]7[{PTiW11O39}2OH]

(PW11Ti)2O:

[Bu4N]8[{PTiW11O39}2O]

PW11TiOH:

[Bu4N]4[PTi(L)W11O39]

PW11TiOMe:

[Bu4N]4 [PTi(OMe)W11O39]

PW11TiOAr:

[Bu4N]4[PTi(OAr)W11O39], ArOH = TMP

PW11Ti = O:

[Bu4N]5 [PTi(O)W11O39]

I:

[Bu4N]4[HPTi(O2)W11O39]

II:

[Bu4N]5[PTi(O2)W11O39]

III:

[H2PTi(O2)W11O39]3-

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    Oxana A. Kholdeeva

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Kholdeeva, O.A. Titanium-monosubstituted polyoxometalates: relation between homogeneous and heterogeneous Ti-single-site-based catalysis. Top Catal 40, 229–243 (2006). https://doi.org/10.1007/s11244-006-0124-4

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