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Synthesis and characterization of azo-linked Schiff bases and their nickel(II), copper(II), and zinc(II) complexes

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Abstract

Azo compounds were prepared by coupling of benzenediazonium chloride ions with 1-amino-2-hydroxy-4-naphthalene sulfonic acid under alkaline conditions, and Schiff bases, L1–3 were then obtained by the condensation of 1-amino-2-hydroxy-3-(phenylazo)-4-naphthalene sulfonic acid, 1-amino-2-hydroxy-3-(4-ethylphenylazo)-4-naphthalene sulfonic acid, and 1-amino-2-hydroxy-3-(4-nitrophenylazo)-4-naphthalene sulfonic acid with salicylaldehyde. New copper(II), nickel(II), and zinc(II) complexes of the Schiff base ligands were also prepared and characterized by spectroscopic methods, magnetic measurements, elemental, and thermogravimetric analysis.

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Authors and Affiliations

  1. Department of Chemistry, Pamukkale University, Kinikli Campus, 20017, Denizli, Turkey

    Emin Erdem, Eylem Yildirim Sari, Rafet Kilinçarslan & Nilgün Kabay

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  1. Emin Erdem
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  2. Eylem Yildirim Sari
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  3. Rafet Kilinçarslan
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  4. Nilgün Kabay
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Correspondence to Rafet Kilinçarslan.

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Erdem, E., Sari, E.Y., Kilinçarslan, R. et al. Synthesis and characterization of azo-linked Schiff bases and their nickel(II), copper(II), and zinc(II) complexes. Transition Met Chem 34, 167–174 (2009). https://doi.org/10.1007/s11243-008-9173-9

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