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Macrocyclic metal complexes: synthesis and characterization of 14- and 16- membered tetraaza macrocyclic complexes of transition metals

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Abstract

A new 14-membered macrocyclic ligand, 5,7,12,14-dibenzo-2,3,9,10-tetraoxa-1,4,8,11-tetraazacyclotetradecane and a 16-membered ligand, 6,8,14,16-dibenzo-4,12-dimethyl-2,10-diphenyl-1,5,9,13-tetraazacyclohexadeca-1,5,9,12-tetra-ene and their transition metal complexes were prepared by the template method and characterized on the basis of elemental analysis, i.r., 1H-n.m.r., electronic spectral studies, conductivity and magnetic susceptibility measurements.

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Authors and Affiliations

  1. Department of Chemistry, Indian Institute of Technology, Roorkee, 247667, India

    Ashok Kumar Singh, Rupam Singh & Puja Saxena

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  1. Ashok Kumar Singh
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  2. Rupam Singh
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  3. Puja Saxena
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Singh, A.K., Singh, R. & Saxena, P. Macrocyclic metal complexes: synthesis and characterization of 14- and 16- membered tetraaza macrocyclic complexes of transition metals. Transition Met Chem 29, 867–869 (2004). https://doi.org/10.1007/s11243-004-1732-0

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  • DOI: https://doi.org/10.1007/s11243-004-1732-0

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