Skip to main content
Log in

Structure and Properties of Nanocrystalline Iron Oxide Powder Prepared by the Method of Pulsed Laser Ablation

  • Published:
Russian Physics Journal Aims and scope

Colloidal solution of iron oxide nanoparticles is synthesized by nanosecond pulsed laser ablation (Nd:YAG laser, 1064 nm, 7 ns, and 180 mJ) of a metallic iron target in water, and nanocrystalline powder is prepared from this solution by vacuum drying. A composition and structure of the material obtained are investigated by methods of electron microscopy, x-ray diffraction, and optical spectroscopy. It is established that oxide particles with average size of about 5 nm and Fe3O4 magnetite structure are mainly formed during ablation. Preliminary investigation of magnetic properties of the prepared nanoparticle powders shows that they can be in ferromagnetic and/or superparamagnetic states.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. E. Vahabzadeh and M. J. Torkamany, J. Clust. Sci., 25, 959–968 (2014).

    Google Scholar 

  2. C. Baker, S. Ismat Shah, and S. K. Hasanain, J. Magn. Magn. Mater., 280, 412–418 (2004).

    Article  ADS  Google Scholar 

  3. G. F. Goya, T. S. Berquo, F. C. Fonseca, et al., J. Appl. Phys., 94, 3520–3527 (2003).

    Article  ADS  Google Scholar 

  4. M. V. Yigit, D. Mazumdar, and Y. Lu, Bioconjugate Chem., 19, 412–417 (2008).

    Article  Google Scholar 

  5. M. K. Yu, D. Kim, I.-H. Lee, et al., Small, 7, 2241–2249 (2011).

    Article  Google Scholar 

  6. S. Kayal and R. V. Ramanujan, J. Nanosci. Nanotech., 10, 5527–5539 (2010).

    Google Scholar 

  7. P. D. Kim, S. S. Zamay, T. N. Zamay, et al., Dokl. Biochem. Biophys., 466, 66–69 (2016).

    Article  Google Scholar 

  8. R. A. Ismail, G. M. Sulaiman, S. A. Abdulrahman, et al., Mater. Sci. Eng., 53, 286–297 (2015).

    Article  Google Scholar 

  9. S. Kalyani, J. Sangeetha, and J. Philip, J. Nanosci. Nanotech., 15, 5768–5774 (2015).

    Google Scholar 

  10. C. Baker, S. Ismat Shah, and S. K. Hasanain, J. Magn. Magn. Mater., 280, 412–418 (2004).

    Article  ADS  Google Scholar 

  11. H. Xia, J. Wang, Y. Tian, et al., Adv. Mater., 22, 3204–3207 (2010).

    Article  Google Scholar 

  12. V. A. Svetlichnyi and I. N. Lapin, Russ. Phys. J., 56, 581–587 (2013).

    Article  Google Scholar 

  13. V. A. Svetlichnyi and I. N. Lapin, Russ. Phys. J., 57, 1789–1792 (2014).

    Article  Google Scholar 

  14. I. N. Lapin and V. A. Svetlichnyi, Proc. SPIE, 9810, 98100T (7 pp.) (2015).

    Article  ADS  Google Scholar 

  15. O. N. Shebanova and P. Lazor, J. Raman Spectrosc., 34, 845–852 (2003).

    Article  ADS  Google Scholar 

  16. D. A. Velikanov, Vibrating sample magnetometer, RF Patent No. 2339965 (Publ. November 27, 2008, Bull. No. 33).

  17. D. A. Velikanov, Vibrating sample magnetometer, RF Patent No. 2341810 (Publ. November 27, 2008, Bull No. 35).

  18. Y.-S. Li, J. S. Church, and A. L. Woodhead, J. Magn. Magn. Mater., 324, 1543–1550 (2012).

    Article  ADS  Google Scholar 

  19. D. L. A. De Faria, S. Venancio Silva, and M. T. de Oliveira, J. Raman Spectrosc., 28, 873–878 (1997).

    Article  ADS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to V. A. Svetlichnyi.

Additional information

Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 12, pp. 30–34, December, 2016.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Svetlichnyi, V.A., Shabalina, A.V. & Lapin, I.N. Structure and Properties of Nanocrystalline Iron Oxide Powder Prepared by the Method of Pulsed Laser Ablation. Russ Phys J 59, 2012–2016 (2017). https://doi.org/10.1007/s11182-017-1008-8

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11182-017-1008-8

Keywords

Navigation