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Synthesis and properties of lead nanoparticles

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Abstract

Lead nanoparticles were synthesized by the thermal decomposition of lead stearate in octanol. The nanoparticles were characterized by X-ray powder diffraction, thermal analysis, IR spectroscopy, and electron microscopy. The lead particle size can be controlled by both varying the concentration of lead stearate in octanol and changing the thermolysis time. Lead nanoparticles have an organic coat composed of decomposition products of lead stearate. This coat prevents the particles from oxidation in air and favors their dissolution in organic solvents.

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Authors and Affiliations

  1. Tomsk Polytechnic University, 30 prosp. Lenina, 634050, Tomsk, Russian Federation

    D. V. Akimov, N. B. Egorov, I. I. Zherin & V. F. Usov

  2. V. E. Zuev Institute of Atmospheric Optics of Siberian Branch of the Russian Academy of Science, 1 pl. Akad. Zueva, 634021, Tomsk, Russian Federation

    O. S. Andrienko

Authors
  1. D. V. Akimov
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  2. O. S. Andrienko
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  3. N. B. Egorov
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  4. I. I. Zherin
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  5. V. F. Usov
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Corresponding author

Correspondence to N. B. Egorov.

Additional information

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 2, pp. 225–229, February, 2012.

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Akimov, D.V., Andrienko, O.S., Egorov, N.B. et al. Synthesis and properties of lead nanoparticles. Russ Chem Bull 61, 225–229 (2012). https://doi.org/10.1007/s11172-012-0032-7

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  • DOI: https://doi.org/10.1007/s11172-012-0032-7

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