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Trinuclear zinc β-naphthoate complexes: synthesis and structure

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Abstract

New trinuclear ZnII β-naphthoate complexes with mono- and bidentate N-donor ligands (2,3-lutidine (lut), 1,10-phenanthroline (phen), and 5,5′-di-tert-butyl-2,2′-bipyridine (dtb-bpy)), (lut)2Zn3(μ2,η2-OOCR)2(μ2-OOCR)4 (1), [(phen)2Zn3(μ2,η2-OOCR)2(μ2-OOCR)4]·2MeCN··2C6H6 (2), and (dtb-bpy)2Zn3(μ2,η2-OOCR)2(μ2-OOCR)4 (3) (RCOO− is the anion of β-naphthoic acid C10H7COOH), were synthesized. The structures of compounds 1–3 were studied by single-crystal X-ray diffraction. In the crystal structures, molecules 1–3 are ordered due to the coplanar arrangement of the aromatic substituents of the acid and the N-donor ligands, as well as through stacking interactions.

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Authors and Affiliations

  1. N. S. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 31 Leninsky prosp., 119991, Moscow, Russian Federation

    A. E. Goldberg, M. A. Kiskin, A. A. Sidorov & I. L. Eremenko

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  1. A. E. Goldberg
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  2. M. A. Kiskin
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  3. A. A. Sidorov
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  4. I. L. Eremenko
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Corresponding author

Correspondence to M. A. Kiskin.

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Dedicated to Academician V. N. Charushin on the occasion of his 60th birthday.

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 5, pp. 829–834, May, 2011.

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Goldberg, A.E., Kiskin, M.A., Sidorov, A.A. et al. Trinuclear zinc β-naphthoate complexes: synthesis and structure. Russ Chem Bull 60, 849–854 (2011). https://doi.org/10.1007/s11172-011-0133-8

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  • DOI: https://doi.org/10.1007/s11172-011-0133-8

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