Skip to main content
SpringerLink
Log in

Visible light motivated synthesis of polyhydroquinoline derivatives using CdS nanowires

  • Published:
Research on Chemical Intermediates Aims and scope Submit manuscript

Abstract

In this article, we report the synthesis of one-dimensional cadmium sulphide nanowires (CdS NWs) by chemical synthesis approach. These as-synthesized materials were characterized by ultraviolet–visible spectroscopy, X-ray diffraction, scanning electron microscopy with energy dispersive spectroscopy, and transmission electron microscopy analysis. These nanowires have an average diameter of ~20 nm and length up to several micrometres. CdS NWs are highly stability and are found to be a very efficient recyclable/reusable (minimum four times without any significant loss) photocatalyst for polyhydroquinoline synthesis under visible light (Halogen lamp, 70 W) at room temperature. This system offers a mild, efficient, and highly economical alternative to the existing protocols in its catalytic activity under visible light irradiation (λ ≥ 420 nm). These findings will open up new opportunities for developing low-cost efficient photocatalyst synthesis of value added intermediates.

Graphical abstract

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Scheme 1

Similar content being viewed by others

References

  1. N. Zhang, S. Liu, Y.J. Xu, Nanoscale 4, 2227 (2012)

    Article  CAS  Google Scholar 

  2. M.R. Hoffmann, S.T. Martin, W. Choi, D.W. Bahnemann, Chem. Rev. 95, 69 (1995)

    Article  CAS  Google Scholar 

  3. P.V. Kamat, J. Phys. Chem. C 111, 2834 (2007)

    Article  CAS  Google Scholar 

  4. X. Chen, S.S. Mao, Chem. Rev. 107, 2891 (2007)

    Article  CAS  Google Scholar 

  5. F. Maldotti, A. Molinari, R. Amadelli, Chem. Rev. 102, 3811 (2002)

    Article  CAS  Google Scholar 

  6. D. Jiang, Z. Sun, H. Jia, D. Lu, P. Du, J. Mater. Chem. A 4, 675 (2016)

    Article  CAS  Google Scholar 

  7. T. Hisatomi, J. Kubot, K. Domen, Chem. Soc. Rev. 43, 7520 (2014)

    Article  CAS  Google Scholar 

  8. Y. Ma, X. Wang, Y. Jia, X. Chen, H. Han, C. Li, Chem. Rev. 114, 998 (2014)

    Article  Google Scholar 

  9. J. Wu, Z. Lan, J. Lin, M. Huang, Y. Huang, L. Fan, G. Luo, Chem. Rev. 115, 2136 (2015)

    Article  CAS  Google Scholar 

  10. R. Chauhan, A. Kumar, R.P. Chaudhar, Res. Chem. Intermed. 39, 645 (2013)

    Article  CAS  Google Scholar 

  11. H. Tada, T. Kiyonaga, S. Naya. Chem. Soc. Rev. 38, 1849 (2009)

    Article  CAS  Google Scholar 

  12. M.A. Fox, Acc. Chem. Res. 16, 314 (1983)

    Article  CAS  Google Scholar 

  13. R.R. Harale, P.V. Shitre, B.R. Sathe, M.S. Shingare, Res. Chem. Intermed. 42, 6695 (2016)

    Article  CAS  Google Scholar 

  14. P.V. Shitre, R.R. Harale, B.R. Sathe, M.S. Shingare, Res. Chem. Intermed. (2016). doi:10.1007/s11164-016-2667-8

    Google Scholar 

  15. C.J. Barrelet, Y. Wu, D.C. Bell, C.M. Lieber, J. Am. Chem. Soc. 125, 11498 (2003)

    Article  CAS  Google Scholar 

  16. J.S. Jang, U.A. Joshi, J.S. Lee, J. Phys. Chem. C 111, 13280 (2007)

    Article  CAS  Google Scholar 

  17. P. Yan, Y. Xie, Y. Qian, X. Liu, Chem. Commun. 1293, 32 (1999)

    Google Scholar 

  18. W. Qingqing, X. Gang, H. Gaorong, J. Solid State Chem. 178, 2680 (2005)

    Article  Google Scholar 

  19. B. Weng, S. Liu, N. Zhang, Z.R. Tang, Y.J. Xu, J. Catal. 309, 146 (2014)

    Article  CAS  Google Scholar 

  20. S. Liu, C. Han, Z.R. Tang, Y.J. Xu, Mater. Horiz. 3, 270 (2016)

    Article  CAS  Google Scholar 

  21. C. Han, N. Zhang, Y.J. Xu, Nano Today 11, 351 (2016)

    Article  CAS  Google Scholar 

  22. M.Q. Yang, Y.J. Xu, Phys. Chem. Chem. Phys. 15, 19102 (2013)

    Article  CAS  Google Scholar 

  23. G. Swarnalatha, G. Prasanthi, N. Sirisha, C.C. Madhusudhana, Int. J. Chem. Tech. Res. 3, 75 (2011)

    CAS  Google Scholar 

  24. S.S. Mansoor, K. Aswin, K. Logaiya, S.P.N. Sudhan, Arab. J. Chem. (2013). doi:10.1016/j.arabjc.2012.10.017

    Google Scholar 

  25. S. Ko, M.N.V. Sastry, C. Lin, C.F. Yao, Tetrahedron Lett. 46, 5771 (2005)

    Article  CAS  Google Scholar 

  26. H. Adibi, H.A. Samimi, M. Beygzadeh, Catal. Commun. 8, 2119 (2007)

    Article  CAS  Google Scholar 

  27. N.N. Karade, V.H. Budhewara, S.V. Shinde, W.N. Jadhav, Lett. Org. Chem. 4, 16 (2007)

    Article  CAS  Google Scholar 

  28. S. Ko, C.F. Yao, Tetrahedron 62, 7293 (2006)

    Article  CAS  Google Scholar 

  29. M.M. Heravi, K.N. Bakhtiri, M. Javadi, F.F. Bamoharram, M. Saeedi, H.A. Oskooi, J. Mol. Catal. A 264, 50 (2007)

    Article  CAS  Google Scholar 

  30. J.L. Donelson, A. Gibbs, S.K. De, J. Mol. Catal. A Chem. 256, 309 (2006)

    Article  CAS  Google Scholar 

  31. A. Kumar, R.A. Maurya, Tetrahedron Lett. 48, 3887 (2007)

    Article  CAS  Google Scholar 

  32. S.R. Cherkupally, R. Mekalan, Chem. Pharm. Bull. 56, 1002 (2008)

    Article  CAS  Google Scholar 

  33. G. Sabitha, G.S.K. Reddy, C.S. Reddy, J.S. Yadav, Tetrahedron Lett. 44, 4129 (2003)

    Article  CAS  Google Scholar 

  34. L.M. Wang, J. Sheng, J.W. Zhang, J.W. Han, Z.Y. Fan, H. Tian, C.T. Qian, Tetrahedron 61, 1539 (2005)

    Article  CAS  Google Scholar 

  35. R. Ranjbar-Karimi, S. Hashemi-Uderji, A. Bazmandegan Shamili, Chin. J. Chem. 29, 1624 (2011)

    Article  CAS  Google Scholar 

  36. M. Nasr-Esfahani, S.J. Hoseini, M. Montazerozohori, R. Mehrabi, H. Nasrabadi, J. Mol. Catal. A Chem. 38, 299 (2014)

    Google Scholar 

  37. S. Das, S. Samanta, S.K. Maji, P.K. Samanta, A.K. Dutta, D.N. Srivastava, B. Adhikary, P. Biswas, Tetrahedron Lett. 51, 1090 (2013)

    Article  Google Scholar 

  38. K. Pal, Uday N. Maiti, T.P. Majumder, S.C. Debnath, Appl. Surf. Sci. 258, 163 (2011)

    Article  CAS  Google Scholar 

  39. Xin Zhang, Nan Zhang, Yi-Jun Xuab, Zi-Rong Tang, New J. Chem. 39, 6756 (2015)

    Article  CAS  Google Scholar 

  40. Z. Zarnegar, J. Safari, Z.M. Kafroudi, New J. Chem. 39, 1445 (2015)

    Article  CAS  Google Scholar 

  41. S.B. Sapkal, K.F. Shelke, B.B. Shingate, M.S. Shingare, Tetrahedron Lett. 50, 1754 (2009)

    Article  CAS  Google Scholar 

  42. S.U. Tekale, V.P. Pagore, S.S. Kauthale, R.P. Pawar, Chin. Chem. Lett. 25, 1149 (2014)

    Article  CAS  Google Scholar 

  43. M.A. Chari, K. Syamasundar, Catal. Commun. 6, 624 (2005)

    Article  Google Scholar 

  44. A. Mobinikhaledi, N. Foroughifar, M.A. Bodaghi Fard, H. Moghanian, S. Ebrahimi, M. Kalhor, Synth. Commun. 39, 1166 (2009)

    Article  CAS  Google Scholar 

  45. Y.L.N. Murthy, A. Rajack, M.T. Ramji, J.J. Babu, C. Praveen, K.A. Lakshmi, Bioorg. Med. Chem. Lett. 22, 6016 (2012)

    Article  CAS  Google Scholar 

  46. C.S. Reddy, M. Raghu, Chem. Pharm. Bull. 56, 1002 (2008)

    Article  Google Scholar 

  47. S. Ko, M.N.V. Sastry, C. Lin, C.F. Yao, Tetrahedron Lett. 46, 5771 (2005)

    Article  CAS  Google Scholar 

  48. B.P. Bandgar, P.E. More, V.T. Kamble, J.V. Totre, Arkivoc 15, 1 (2008)

    Google Scholar 

  49. A. Debache, W. Ghalem, R. Boulcina, A. Belfaitah, S. Rhouati, B. Carboni, Tetrahedron Lett. 50, 5248 (2009)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

An Emeritus Scientist Fellowship awarded to M.S.S. by the Council of Scientific and Industrial Research, New Delhi (Project vide No. 21(0919)/12/EMR-II Dated 25-04-2013) is gratefully acknowledged. One of the authors, R.R.H., is thankful to CSIR, New Delhi, India, for financial assistance in the form of Senior Research Fellowship. Authors are also grateful to the Department of Chemistry, Dr. B. A. Marathwada University, Aurangabad, for providing the laboratory facilities. We also thank SAIF Divisions of IIT Bombay and CDRI, Lucknow, for providing analytical data.

Author information

Authors and Affiliations

  1. Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, 431004, India

    Rajkumar R. Harale, Praveen V. Shitre, Bhaskar R. Sathe & Murlidhar S. Shingare

Authors
  1. Rajkumar R. Harale
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Praveen V. Shitre
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Bhaskar R. Sathe
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Murlidhar S. Shingare
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Murlidhar S. Shingare.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Harale, R.R., Shitre, P.V., Sathe, B.R. et al. Visible light motivated synthesis of polyhydroquinoline derivatives using CdS nanowires. Res Chem Intermed 43, 3237–3249 (2017). https://doi.org/10.1007/s11164-016-2822-2

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11164-016-2822-2

Keywords

Search

Navigation