Abstract
Gelatin-stabilized gold nanoparticles (AuNPs-gelatin) with controlled particle size were synthesized with simple variation of concentration of gelatin by reducing in situ tetrachloroauric acid with sodium citrate. The nanoparticles showed excellent colloidal stability. Transmission electron microscopy (TEM) revealed the formation of well-dispersed gold nanoparticles (AuNPs) with different sizes. The methodology produces particles 10–15 nm in size depending on the concentration of gelatin used. The measured AuNPs are 10, 11, 12, 13, 14, and 15 nm for AuNPs-gelatin 1, 0.5, 0.25, 0.1 and 0.05%, and pure AuNPs, respectively. The AuNPs-gelatin exhibit size-dependent localized surface plasmon resonance behavior as measured by UV–visible spectroscopy. UV–vis spectroscopy and TEM results suggest that higher concentration of gelatin favor smaller particle size and vice versa. FTIR spectroscopy analysis of AuNPs-gelatin revealed the amino bands and carboxyl peak of gelatin. The crystalline nature of AuNPs was investigated by X-ray diffraction.
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Acknowledgments
This work was financially supported by the Korea Science & Engineering Foundation (KOSEF) grant funded by the Korea government (MOST) (No. R01-2007-000-20488-0) and Brain Korea 21 project, Chonbuk National University. Authors wish to thanks Mr. Jong Gyun Kang for taking good quality TEM images.
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Neupane, M.P., Lee, S.J., Park, I.S. et al. Synthesis of gelatin-capped gold nanoparticles with variable gelatin concentration. J Nanopart Res 13, 491–498 (2011). https://doi.org/10.1007/s11051-010-9971-9
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DOI: https://doi.org/10.1007/s11051-010-9971-9