FGUP VIAM has developed technology for melting high-temperature composite material based on the Nb–Si system by vacuum induction melting in a ceramic crucible based on yttrium oxide operating at a melting temperature of more than 2000°C and chemically resistant during melting a highly active composite. This technology makes it possible to prepare billets for directional crystallization of the required geometric dimensions, ensuring a homogeneous chemical composition close to that calculated, and a low impurity content, in particular oxygen.
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Notes
Directional crystallization was accomplished under the leadership of Yu. A. Bondarenko.
The microstructure was studied by V. G. Kolodochkina.
References
N. V. Petrushin, I. L. Svetlov, and O. G. Ospennikova, “Casting nickel-base superalloys,” Vse Materialy. Éntsik. Splav¸ No. 5, 15–19, No. 6, 18-21 (2012).
E. N. Kablov, I. L. Svetlov, and I. Yu. Efimochkin, “High-temperature Nb–Si components,” Vestn. N. E. Bauman NGTU, Ser. Mashin., No. Sp.2, 164–173 (2011).
E. N. Kablov, I. L. Svetlov, M. I. Karpov, et al., “High-temperature composites on the Nb–Si system reinforced with niobium silicide,” Materialoved., No. 2, 24–32 (2017).
E. N. Kablov, I. L. Svetlov, M. I. Karpov, et al., “High-temperature composites based on the Nb–Si system reinforced with niobium silicides,” Inorganic Materials: Applied Research,8, No. 4, 609–617 (2017).
E. N. Kablov, B. S. Lomberg, and O. G. Ospennikova, “Creation of contemporary heat-resistant materials and their manufacturing technology for aero engine building,” Krylya Rodiny, No. 3-4, 34–38 (2012).
D. S. Kashin and P. A. Stekhov, “Protective coatings for heat-resistant alloys based on niobium,” Trudy VIAM Élektron. Nauch. Tekhn. Zh., No. 6, Art. 01, (2015); URL: http://www.viam-works.ru (access date 15.02.2019).
Bowen Xi, C. Changchun, and W. Zhenjun, “Microstructures of Nb/Nb5Si3 composites and it alloyed with W, Mo and W–Mo fabricated by spark plasma sintering,” J. of Alloys and Compounds,583, 574–577 (2010).
H. Yafang, L. Jupin, X. Chengbo, and Z. Xiaoqin, “Mechanical properties and microstructure of Nb/Nb5Si3 /Cr2Nb alloys prepared by spark plasma sintering,” Mater. Sci. Forum,747–748, 747–753 (2013).
L.Yu. Udoeva, A. V. Larionov, N. I. Sel’menskikh, et al., “Phase formation in Nb–Si alloys of eutectic composition alloyed with yttrium,” Privolzh. Nauch. Vestn., No. 1(29), 27–32 (2014).
I. L. Svetlov, Yu. A. Abuzin, B. N. Babich, et al., “High-temperature Nb-Si composites strengthened with niobium silicide,” Zh. Funct. Mater.,1, No. 2, 48–52 (2007).
M. I. Karpov, V. I. Vnukov, V. P. Korzhov, et al., “Structure and mechanical properties of heat-resistant alloy of the Nb–Si system of eutectic composition prepared by directional crystallization,” Deform. Razrush. Materialov., No. 12, 2–8 (2012).
G. Jie, T. Panos, and Sh. Guosheng, “Oxidation of Nb–Si–Cr–Al in situ composites with Mo, Ti and Hf additions,” Mater. Sci. and Eng.,A 441, 26–38 (2006).
Y. Yuncheng, D. Hongsheng, K. Yongwang, and S. Jinxia, “Microstructure evolution and mechanical properties of Nb–Si based alloy processed by electromagnetic cold crucible directional solidification,” Materials and Design,55, 450–455 (2014).
D. Fei, J. Lina, Yu. Sainan, et al., “Microstructure evolution of a hypereutectic Nb–Ti–Si–Cr–Al–Hf alloy processed by directional solidification,” Chinese J. of Aeronautics, 2 Aug. (2013).
L. M. Ma, S. N. Yuan, R. J. Cui, et al., “Interactions between Nb silicide based alloy and yttria mould during directional solidification,” Int. J. of Refractory Metals and Hard Materials,30, 96–101 (2012).
E. N. Kablov, V. V. Sidorov, D. E. Kablov, and P. G. Min, “Metallurgical bases of providing high quality for single-crystal heatresistant alloys,” Aviats. Mater. Tekhnol., No. S, 55–71 (2017).
E. N. Kablov, V. V. Sidorov, D. E. Kablov, et al., “Resource saving technology for melting prospective cast and deformable super high-strength alloys taking account of reprocessing of all forms of waste,” Élektrometall., No. 9, 30–41 (2016).
P. G. Min, V. E. Vadeev, V. P. Piskorskii, and V. V. Kramer, “Development of technology for melting alloys of the REM–Fe–Co–B system with high purity for thermally stable magnets,” Trudy VIAM Élektron Nauch. Tekhn. Zh., No. 21, 3–9 (2016); URL: http://www.viam-works.ru (access date 15.02.2019).
M. Gao, L. Jia, X. Tang, et al., “Interaction mechanism between niobium-silicide-based alloy melt and Y2O3 refractory crucible in vacuum induction melting process,” China Foundry,8, No. 2, 190–196 (2011).
D. E. Kablov, V. V. Sidorov, and P. G. Min, “Effect of nitrogen impurity on the structure of single-crystal nickel-base superalloy ZhS30-VI and development of effective refining methods,” Aviats. Mater. Tekhnol., No. 2, 32–36 (2012).
E. N. Kablov, “Innovative development of FGUP VIAM GNTs RF for implementing strategic areas of material development and technology for processing in the period up to 2030,” Aviats. Mater. Tekhnol., No. 1(34), 3–33 (2015).
I. L. Svetlov, N. A. Kuz’mina, and A. V. Neiman, “Microstructure of Ni/Ni3Al-NbC and niobium Nb-Nb5Si3 eutectic composites,” Materialoved., No. 3, 50–56 (2015).
RF Patent 2618038, МPК C22C 1/02 (2006.01), C22B 9/22 (2006.01), C22C 27/02 (2006.01). Method for preparing heat-resistant alloy based on niobium, Claim 13.10.2015; Publ. 05.02.2017. Bull. No. 13.
RF Patent 2595084, No. 2015108377/02. Method for preparing heat-resistant alloy based on a niobium matrix with intermetallic strengthening, Claim 03.11.2015; Publ. 08.20.2016. Bull. No. 23.
RF Patent 2595084, No. 2015108377/02. Method for preparing heat-resistant alloy based on a niobium matrix with intermetallic strengthening, Claim 03.11.2015; Publ. 08.20.2016. Bull. No. 23.
Yu. A Bondarenko, M. Yu. Kolodyazhnyi, A. B. Echin, and A. R. Narskii, “Directional crystallization, structure and properties of natural composite based on Nb-Si eutectic at working temperatures up to 1350°C for GTE blades,” Trudy VIAM Élektron. Nauch. Tekhn. Zh., No. 1, Art. 1 (2018); URL: http://www.viam-works.ru (access date 15.02.2019).
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Translated from Metallurg, Vol. 63, No. 8, pp. 91–96, August, 2019.
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Min, P.G., Vadeev, V.E. Vacuum Induction Furnace Melting Technology for High-Temperature Composite Material Based on Nb–Si System. Metallurgist 63, 878–884 (2019). https://doi.org/10.1007/s11015-019-00902-y
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DOI: https://doi.org/10.1007/s11015-019-00902-y