Summary
The SCTA methods for the kinetic analysis of solid-state reactions have been reviewed. It has been shown that these methods present two important advantages with regards to the more conventional rising temperature experiments. Firstly, they have a higher resolution power for discriminating among the reaction kinetic models and, secondly, SCTA is a powerful tool for minimizing the influence of the experimental conditions on the forward reaction.
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Criado, J., Pérez-Maqueda, L. Sample controlled thermal analysis and kinetics. J Therm Anal Calorim 80, 27–33 (2005). https://doi.org/10.1007/s10973-005-0609-6
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DOI: https://doi.org/10.1007/s10973-005-0609-6