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Thermal stability of ZrO2–SiO2 aerogel modified by Fe(III) ion

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Abstract

ZrO2–SiO2 aerogel modified by Fe(III) ion was prepared and the stability of the samples under high temperature was investigated. The structure and properties of modified aerogels were characterized by N2 adsorption–desorption, FT-IR, XRD and TEM. The samples still contain a specific surface area about 228 m2/g after 1,000 °C 0.5 h calcinations. The inhibition of ZrO2 particle growth is attributed to the Fe(III) ion modified aerogel surface, which strongly retards the ZrO2 tetragonal phase transformation as well.

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Acknowledgments

This study was supported by the National Natural Science Foundation of China (Grant No. 51172157).

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Authors and Affiliations

  1. Key Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials Science and Engineering, Tianjin University, Tianjin, 300072, People’s Republic of China

    Rui Xiong, Xiaolei Li, Huiming Ji, Xiaohong Sun & Jian He

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  1. Rui Xiong
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  2. Xiaolei Li
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  3. Huiming Ji
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  4. Xiaohong Sun
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  5. Jian He
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Correspondence to Xiaolei Li.

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Xiong, R., Li, X., Ji, H. et al. Thermal stability of ZrO2–SiO2 aerogel modified by Fe(III) ion. J Sol-Gel Sci Technol 72, 496–501 (2014). https://doi.org/10.1007/s10971-014-3464-8

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  • DOI: https://doi.org/10.1007/s10971-014-3464-8

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