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Synthesis of organized mesoporous γ-alumina templated with polymer–colloidal complex

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Abstract

Mesoporous γ-Al2O3 materials with high surface area and a narrow pore size distribution were synthesized by facile sol–gel procedure with application of the polymer–colloid complex as a template.

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Notes

  1. Characterization of the samples: BET surface areas of the samples were calculated from nitrogen physisorption data collected on a Quantachrome Nova 1200 Series-e analyzer at 77 K. The pore size distributions were calculated using the BJH method from the desorption branch of the isotherms. XRD measurements were performed using a Bruker Nanostar U diffractometer using Cu Ka radiation (1.54 Å). The size distribution were measured by dynamic light scattering (DLS, Malvern, Zetasizer nano ZS).

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Acknowledgment

This work is supported by RFBR grant No. 09-03-97553, joint RFBR-DST grant 10-03-92658 and grant of Russian Ministry of Education and Science No. 14.740.12.0862.

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Authors and Affiliations

  1. Institute of Solution Chemistry, Russian Academy of Sciences, 153045, Ivanovo, Russian Federation

    V. V. Vinogradov & A. V. Agafonov

  2. Ivanovo State University of Chemistry and Technology, 153000, Ivanovo, Russian Federation

    A. V. Vinogradov

  3. Fuel Chemistry Division, Bhabha Atomic Research Centre, Mumbai, 400 085, India

    K. T. Pillai, Rajesh V. Pai, S. K. Mukerjee & S. K. Aggarwal

Authors
  1. V. V. Vinogradov
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  2. A. V. Agafonov
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  3. A. V. Vinogradov
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  4. K. T. Pillai
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  5. Rajesh V. Pai
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  6. S. K. Mukerjee
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  7. S. K. Aggarwal
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Correspondence to A. V. Vinogradov.

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Vinogradov, V.V., Agafonov, A.V., Vinogradov, A.V. et al. Synthesis of organized mesoporous γ-alumina templated with polymer–colloidal complex. J Sol-Gel Sci Technol 60, 6–10 (2011). https://doi.org/10.1007/s10971-011-2543-3

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  • DOI: https://doi.org/10.1007/s10971-011-2543-3

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