Abstract
Mesoporous TiO2 with a high specific surface area was prepared from titanium sulfate solution in a simple sol–gel route, where formamide was used as pH adjusting agent. TiO2 had a high resistance to phase transformation, and maintained monophasic anatase after calcinating at 600 °C. The highest specific surface area achieved on the prepared samples is 231.90 m2 g−1 after calcinating at 450 °C.
References
Caamal-Parra AR, Medina-Esquivel RA, Lopez T et al (2007) J Non-Cryst Solids 353:971. doi:10.1016/j.jnoncrysol.2006.12.065
Senthilkumaar S, Porkodi K, Vidyalakshmi R (2005) J Photoch Photobio A 170:225. doi:10.1016/j.jphotochem.2004.07.005
Wang WD, Serp P, Kalck P et al (2005) Appl Catal B-Environ 56:305. doi:10.1016/j.apcatb.2004.09.018
Huo YN, Zhu J, Li JX et al (2007) J Mol Catal Chem 278:237. doi:10.1016/j.molcata.2007.07.054
Rella R, Spadavecchia J, Manera MG et al (2007) Sens Actuators B Chem 127:426. doi:10.1016/j.snb.2007.04.048
Dutta PK, Lucia MFD (2006) Sens Actuators B Chem 115:1. doi:10.1016/j.snb.2005.08.020
Faia PM, Furtado CS, Ferreira AJ (2005) Sens Actuators B Chem 107:353. doi:10.1016/j.snb.2004.10.021
Yoo S, Akbar SA, Sandhage KH (2004) Ceram Int 30:1121. doi:10.1016/j.ceramint.2003.12.085
Auten BJ, Lang HF, Chandler BD (2008) Appl Catal B-Environ 81:225. doi:10.1016/j.apcatb.2007.12.012
Ma Z, Overbury SH, Dai S (2007) J Mol Catal Chem 273:186. doi:10.1016/j.molcata.2007.04.007
Grinis L, Dor S, Ofir A et al (2008) J Photoch Photobio A 198:52. doi:10.1016/j.jphotochem.2008.02.015
Yang L, Lin Y, Jia JG et al (2008) Microporous Mesoporous Mater 112:45. doi:10.1016/j.micromeso.2007.09.011
Sirimanne PM (2008) Renew Energ 33:1424. doi:10.1016/j.renene.2007.07.012
Karthikeyan CS, Thelakkat M (2008) Inorg Chim Acta 361:635. doi:10.1016/j.ica.2007.04.033
Antonelli DM, Ying JY (1995) Angew Chem Int Ed Engl 34:2014. doi:10.1002/anie.199520141
Yoo KS, Lee TG, Kim J et al (2005) Microporous Mesoporous Mater 84:211. doi:10.1016/j.micromeso.2005.05.029
Pavasupree S, Suzuki Y, Pivsa-Art S et al (2005) Ceram Int 31:959. doi:10.1016/j.ceramint.2004.10.009
Wang C, Li Q, Wang RD (2004) Mater Lett 58:1424. doi:10.1016/j.matlet.2003.10.006
Kim DS, Kwak S (2007) Appl Catal Gen 323:110. doi:10.1016/j.apcata.2007.02.010
Latt KK, Kobayashi T (2008) Ultrason Sonochem 15:484. doi:10.1016/j.ultsonch.2007.08.001
Liu Y, Li Y, Wang YT et al (2008) J Hazard Mater 150:153. doi:10.1016/j.jhazmat.2007.04.088
Du JM, Liu ZM, Li ZH et al (2005) Microporous Mesoporous Mater 83:19. doi:10.1016/j.micromeso.2005.03.015
Alonso E, Montequi I, Lucas S et al (2007) J Supercrit Fluid 39:453. doi:10.1016/j.supflu.2006.03.006
Jiang D, Xu Y, Hou B et al (2007) J Solid State Chem 180:1787. doi:10.1016/j.jssc.2007.03.010
Acknowledgments
The authors are grateful for the financial support of Chinese National Programs for High Technology Research and Development (no. 2006AA05Z306). The correction of English language by Dr. Yufeng Cheng, Lin Lu and Jianlong Zhou is gratefully acknowledged.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Zhang, X., Li, X., Wu, J. et al. Simple sol–gel route to synthesis of mesoporous TiO2 . J Sol-Gel Sci Technol 51, 1–3 (2009). https://doi.org/10.1007/s10971-009-1984-4
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10971-009-1984-4