Abstract
In this paper, an improvement study on the closed chamber distillation system for recovery of renewable salts from salt wastes containing radioactive rare earth compounds was performed to determine optimum operating conditions. It was very important to maintain the pressure in the distillation chamber below 10 Torr for a high efficiency (salt recovery >99 %) of the salt distillation. This required increasing the salt vaporization and condensation rates in the distillation system. It was confirmed that vaporization and condensation rates could be improved controlling the given temperature of top of the condensation chamber. In the distillation tests of the salt wastes containing rare earth compounds, the operation time at a given temperature was greatly reduced changing the given temperature of top of the condensation chamber from 780 to 700 °C.
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Acknowledgments
This study was performed under the Nuclear R&D Program of the Korean Ministry of Education, Science and Technology.
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Eun, H.C., Cho, Y.Z., Lee, T.K. et al. An improvement study on the closed chamber distillation system for recovery of renewable salts from salt wastes containing radioactive rare earth compounds. J Radioanal Nucl Chem 295, 345–350 (2013). https://doi.org/10.1007/s10967-012-1856-1
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DOI: https://doi.org/10.1007/s10967-012-1856-1