Skip to main content
Log in

Preparation and characterization of Polyvinylbutyral/Graphene Nanocomposite

  • Original Paper
  • Published:
Journal of Polymer Research Aims and scope Submit manuscript

Abstract

Poly (vinylbutyral) (PVB) was synthesized by condensation of poly (vinylalcohol) (PVA) with butyraldehyde. Nanocomposites of PVB with graphene (0.1 to 0.6 wt%) were prepared via solution blending. The structure and properties of prepared compounds were characterized by FT-IR, X-ray diffraction (XRD), thermal gravimetric analysis (TGA), scanning electron microscopy (SEM) and tensile strength tester (TST). The prepared nanocomposites showed considerable thermal and mechanical properties than PVB and showed good toughness and flexibility.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Scheme 1
Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

References

  1. Zhu Y, Murali S, Cai W, Li X, Suk JW, Potts JR, Ruoff RS (2010) Graphene and Graphene Oxide: Synthesis, Properties, and Applications. Adv Mater 22:3906–24

    Article  CAS  Google Scholar 

  2. Geim AK, Novoselov KS (2007) The rise of graphene. Nat Mater 6(3):183–191

    Article  CAS  Google Scholar 

  3. Compton OC, Nguyen SBT (2010) Graphene oxide, highly reduced graphene oxide, and graphene: versatile building blocks for carbon-based materials. Small 6:711–23

    Article  CAS  Google Scholar 

  4. Iijima S (1991) Helical microtubules of graphitic carbon. Nature 354:56–8

    Article  CAS  Google Scholar 

  5. Ajayan PM, Stephan O, Colliex C, Trauth D (1994) Aligned carbon nanotubes in a thin polymer film. Science 265:1212–14

    Article  CAS  Google Scholar 

  6. Boehm HP, Setton R, Stumpp E (1994) Nomenclature and terminology of graphite intercalation. Pure and Applied Chemistry 66(9):1893–1901

    Article  CAS  Google Scholar 

  7. Koo JH (2006) Polymer nanocomposite, Mc Graw-Hill New York

  8. Potts JR, Dreyer DR, Bielawski CW, Ruoff RS (2010) Graphene-based polymer nanocomposites. doi:10.1016/J.Polymer2010.11.042.

  9. Wang J, Wang X, Chunhui X, Zhang M, Shang X (2011) Preparation of graphene/poly(vinyl alcohol) nanocomposites with enhanced mechanical properties and water resistance. Polym Int 60(5):816–822

    Article  CAS  Google Scholar 

  10. Wang J, Huating H, Wang X, Chunhui X, Zhang M, Shang X (2011) Preparation and mechanical and electrical properties of graphene nanosheets–poly(methyl methacrylate) nanocomposites via in situ suspension polymerization. J Appl Polym Sci 122(3):1866–1871

    Article  CAS  Google Scholar 

  11. Rafiee MA, Rafiee J, Wang Z, Song H, Zhong-Zhen Y, Koratkar N (2009) Enhanced Mechanical Properties of Nanocomposites at Low Graphene Content. J Am Chem Soc 3(11):3884–3890

    CAS  Google Scholar 

  12. Staudenmaier L (1898) Verfahren zur Darstellung der Graphitsaure Ber. Dtsch Chem Ges 31:1481–1487

    Article  CAS  Google Scholar 

  13. Staudenmaier L (2006) Verfahren zur Darstellung der Graphitsaure. Eur J Inorg Chem 31(2):1481–1487

    Google Scholar 

  14. Schniepp HC, Li J-L, Mc Allister MJ, Sai H, Herrera-Alonso M, Adamson DH, Prud home RK, Car R, Saville DA, Aksay IA (2006) Functionalized Single Graphene Sheets Derived from Splitting Graphite Oxide. J Phys Chem B 110(170):8535–8539

    Article  CAS  Google Scholar 

Download references

Acknowledgment

The authors would like to appreciate University of Isfahan for supporting this work.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Mohammad Reza Reisi.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Hajian, M., Reisi, M.R., Koohmareh, G.A. et al. Preparation and characterization of Polyvinylbutyral/Graphene Nanocomposite. J Polym Res 19, 9966 (2012). https://doi.org/10.1007/s10965-012-9966-6

Download citation

  • Received:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1007/s10965-012-9966-6

Keywords

Navigation