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Mössbauer Study and Curie Temperature Configuration on Sintering Nano-Ni-Zn Ferrite Powder

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Abstract

Variations of Curie temperature and strength of magnetic phases with sintering temperature and Ni concentration is investigated in the present work. The AC susceptibility studies show a decrease in Curie temperature (TC) with an increase in Ni concentration in the samples. Comparison of Curie temperatures with the reported results reveals that samples in the present work show higher TC enabling high thermal stability. The Mössbauer spectra of nano- and sintered Ni-Zn ferrite samples were recorded at room temperature to monitor the local environment around Fe cations through Mössbauer hyperfine parameters as a function of composition and sintering temperatures. The increase in sharpness of the Mössbauer sextet with an increase in Ni concentration and sintering temperature corroborate improvement in homogeneity and ferrimagnetic ordering. The results of hyperfine parameters offer the possibility of having close view on configuring Curie temperature through monitoring hyperfine field by altering sintering temperature and/or Ni concentration. As the temperature dependence of magnetic and magnetoelastic properties is strongly influenced by the Curie temperature, the successful possible configuration of Curie temperature in the present work can be further investigated for desired sensor applications.

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Authors and Affiliations

  1. Department of Physics, Dnyanprassarak Mandal’s College and Research Centre, Assagao, Bardez, Goa, 403 507, India

    Manoj M. Kothawale

  2. Department of Physics, Goa University, Taleigao Plateau, Goa, 403206, India

    R. B. Tangsali

  3. Solid State Physics Division, Physics Division, Bhabha Atomic Research Centre, Mumbai, 400085, India

    Sher Singh Meena

  4. Department of Metallurgical Engineering, Indian Institute of Technology, Banaras Hindu University, Varanasi, 221005, India

    N. K. Prasad & Asnit Gangwar

Authors
  1. Manoj M. Kothawale
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  2. R. B. Tangsali
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  3. Sher Singh Meena
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  5. Asnit Gangwar
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Correspondence to Manoj M. Kothawale.

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Kothawale, M.M., Tangsali, R.B., Meena, S.S. et al. Mössbauer Study and Curie Temperature Configuration on Sintering Nano-Ni-Zn Ferrite Powder. J Supercond Nov Magn 32, 2141–2147 (2019). https://doi.org/10.1007/s10948-018-4935-x

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