Abstract
The multicomponent substance obtained by laser evaporation of the BN target under nitrogen was studied by X-ray fluorescence and X-ray absorption spectroscopy. The BK α spectra of the substance and boroncontaining compounds rh-BN, B2O3, and α-B were measured on a laboratory instrument using an ethyleneglycol distearate crystal as an analytical element; X-ray absorption spectra near the boron and nitrogen K edge were recorded on a BESSY synchrotron radiation station. The contents of the components in the synthesized substance were evaluated by decomposing the BK α spectrum into the spectra of the test boron-containing compounds. A comparison of the X-ray absorption spectra near the NK edge of the substance and rh-BN revealed that BN nanostructures obtained by laser evaporation were defective.
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References
M. Terrones, J. M. Romo-Herrera, E. Cruz-Silva, et al., Materials Today, 10, 30 (2007).
S. V. Ordin, B. N. Sharupin, and M. I. Fedorov, Fiz. Tekh. Poluprovodn., 32, No. 9, 1033 (1998).
L. Wirtz, A. Rubio, R. Arenal, and A. Loiseau, Phys. Rev. B, 68, 045425 (2003).
L. Wirtz, A. Marini, and A. Rubio, Phys. Rev. Lett., 96, 126104 (2006).
R. S. Lee, J. Gavillet, M. Lamy de la Chapelle, et al., Phys. Rev. B, 64, 121405 (R) (2001).
J. Guo, Int. J. Nanotechn., 1, 193 (2004).
K. Asokan, S. K. Srivastava, D. Kabiraj, et al., Nucl. Instr. Meth., Phys. Res., Sect. B, 193, 324 (2002).
I. M. Arber, P. Norman, D. S. Urch, and D. J. Bloor, J. Cryst. Growth, 84, 145–150 (1987).
A. V. Okotrub, T. A. Duda, D. D. Gaun, et al., Poverkhnost, No. 8, 30 (2003).
T. Kaneyoshi, H. Kohzuki, Y. Muramatsu, et al., X-Ray Spectr., 28, 497 (1999).
Y. Muramatsu, M. Oshima, and H. Kato, Phys. Rev. Lett., 71, No. 3, 44851 (1993).
R. D. Carson and S. E. Schnatterly, ibid., 59, No. 3, 319 (1987).
A. Mansor and S. E. Schnatterly, ibid., No. 5, 567.
A. D. Becke, J. Chem. Phys., 98, 5648 (1993).
C. Lee, W. Yang, and R. G. Parr, Phys. Rev. B, 37, 785 (1988).
Jaguar 3.5, Schrodinger, Inc., Portland, OR (1998).
A. L. Ivanovskii, Usp. Khim., 66, 511 (1997).
T. Hemraj-Benny, S. Banerjee, S. Sambasivan, et al., Phys. Chem. Chem. Phys., 7, 1103 (2005).
H. C. Choi, S. Y. Bae, W. S. Jang, and J. Park, J. Phys. Chem. B, 109, 7007 (2005).
A. Zobelli, C. P. Ewels, A. Gloter, et al., Nanoletters, 6, 1955 (2006).
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Original Russian Text Copyright © 2008 by Yu. V. Lavskaya, T. A. Duda, V. O. Koroteev, A. A. Guzev, V. N. Demin, L. G. Bulusheva, A. V. Okotrub, L. Bresson, and A. Loiseau
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Translated from Zhurnal Strukturnoi Khimii, Vol. 49, Supplement, pp. S44–S50, 2008.
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Lavskaya, Y.V., Duda, T.A., Koroteev, V.O. et al. X-ray spectral study of a material containing BN nanostructures. J Struct Chem 49 (Suppl 1), 40–46 (2008). https://doi.org/10.1007/s10947-008-0199-9
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DOI: https://doi.org/10.1007/s10947-008-0199-9