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Hierarchical macroporous epoxy resin templated from single semi-fluorinated surfactant

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Abstract

A hierarchical macroporous epoxy resin monolith has been successfully synthesized via a single semi-fluorinated surfactant (FSO-100) templating approach. The hierarchical macroporous material is characterized by variety of techniques such as scanning electron microscopy (SEM), transmission electron microscopy (TEM), thermogravimetric (TG), infrared (IR) and X-ray diffraction (XRD). The results show that this material features a hierarchical macropore distribution with pore sizes at 0.4–2 μm and 20–100 nm, respectively. Additionally, the semi-fluorinated surfactant (FSO-100) disperses homogenerously in the epoxy resin, which imparts mesoscopic features.

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Acknowledgments

This work was supported by the National Natural Science Foundation of China (20773049). We gratefully acknowledge Dr. Wei Zhang and Dr. Yi-Jun Xu at the Fritz-Haber-Institute of the Max Planck Society for the help of TEM characterization and discussion, and Dr. Toshiyuki Yokoi, Prof. Takashi Tatsumi in Japan for the help of HR-SEM characterization.

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Authors and Affiliations

  1. State Key Laboratory of Inorganic Synthesis and Preparative Chemistry and College of Chemistry, Jilin University, 130023, Changchun, China

    Yonglai Zhang, Hong Ding, Shu Wei, Sen Liu, Yuanpeng Wang & Feng-Shou Xiao

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  1. Yonglai Zhang
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  2. Hong Ding
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  3. Shu Wei
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  4. Sen Liu
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  5. Yuanpeng Wang
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  6. Feng-Shou Xiao
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Correspondence to Feng-Shou Xiao.

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Zhang, Y., Ding, H., Wei, S. et al. Hierarchical macroporous epoxy resin templated from single semi-fluorinated surfactant. J Porous Mater 17, 693–698 (2010). https://doi.org/10.1007/s10934-009-9340-1

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  • DOI: https://doi.org/10.1007/s10934-009-9340-1

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