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Structural and ferroelectric properties of microwave heated lead cobalt titanate nanoparticles synthesized by sol–gel technique

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Abstract

The lead cobalt titanate (PCT) nanoparticles were prepared by sol–gel method and further microwave heated at 1023 K for 3/4 h. The X-ray diffraction pattern revealed the formation of PCT phases. The average crystallite-size was acquired to be 26.3 nm. The surface morphology of specimen was analyzed using transmission electron microscope. The ferroelectric property was elucidated by means of polarization versus electric field loop as a function of temperature.

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References

  1. G. Wang, R. Sæterli, P.M. Rørvik, A.T. van Helvoort, R. Holmestad, T. Grande, M.-A. Einarsrud, Self-assembled growth of PbTiO3 nanoparticles into microspheres and bur-like structures. Chem. Mater. 19, 2213–2221 (2007)

    Article  Google Scholar 

  2. J. Wang, X. Pang, M. Akinc, Z. Lin, Synthesis and characterization of perovskite PbTiO3 nanoparticles with solution processability. J. Mater. Chem. 20, 5945–5949 (2010)

    Article  Google Scholar 

  3. K. Kanchiang, P. Amonpattaratkit, S. Ananta, Y. Laosiritaworn, Phase formation behavior of perovskite ferroelectric lead zirconate titanate—lead zinc niobate powders by X-ray absorption spectroscopy. Integr. Ferroelectr. 175, 73–80 (2016). https://doi.org/10.1080/10584587.2016.1201390

    Article  Google Scholar 

  4. K.C. Babu Naidu, T.S. Sarmash, M. Maddaiah, A. Gurusampath Kumar, D. Jhansi Rani, V. Sharon Samyuktha, L. Obulapathi, T. Subbarao, Structural and electrical properties of PbO-doped SrTiO3 ceramics. J. Ovonic Res. 11, 79–84 (2015)

    Google Scholar 

  5. K.-Y. Andrew Lin, D.-Y. Lin, Y.-C. Lu, J.-T. Lin, Y.-F. Lin, Electrospun nanofiber of cobalt titanate perovskite as an enhanced heterogeneous catalyst for activating peroxymonosulfate in water. Chem. Eng. Sci. (2017). https://doi.org/10.1016/j.ces.2017.05.013

    Google Scholar 

  6. X. Zhao, Z. Cai, T. Wang, W. O’Reilly, D. Liu, B. Zhao, A new type of cobalt-deposited titanate nanotubes for enhanced photocatalytic degradation of phenanthrene. Appl. Catal. B (2016). https://doi.org/10.1016/j.apcatb.2016.01.010

    Google Scholar 

  7. L. Gianni Ciofania, C. Ricotti, D. Canalec, S. DAlessandrod, B. Berrettini, V. Mazzolai, Mattoli, Effects of barium titanate nanoparticles on proliferation and differentiation of ratmesenchymal stem cells. Colloids Surf. B 102, 312–320 (2013)

    Article  Google Scholar 

  8. K. Chandra Babu Naidu, W. Madhuri, Effect of microwave heat treatment on pure phase formation of hydrothermal synthesized nano NiMg ferrites. Phase Trans. (2017). https://doi.org/10.1080/01411594.2016.1277220

    Google Scholar 

  9. K. Chandra Babu Naidu, S. Roopas Kiran, W. Madhuri, Investigations on transport, impedance and electromagnetic interference shielding properties of microwave processed NiMg ferrites. Mater. Res. Bull. 89, 125–138 (2017)

    Article  Google Scholar 

  10. K. Chandra Babu Naidu, W. Madhuri, Microwave processed NiMg ferrites: studies on structural and magnetic properties. J. Magn. Magn. Mater. 420, 109–116 (2016)

    Article  Google Scholar 

  11. K. Chandra Babu Naidu, W. Madhuri, Microwave assisted solid state reaction method: investigations on electrical and magnetic properties NiMgZn ferrites. Mater. Chem. Phys. 181, 432–443 (2016)

    Article  Google Scholar 

  12. S. Prathap, W. Madhuri, Multiferroic properties of microwave sintered PbFe12–xO19–δ. J. Magn. Magn. Mater. 430 114–122 (2017)

    Article  Google Scholar 

  13. G.-L. Tan, W. Li, Ferroelectricity and ferromagnetism of M-type lead hexaferrites. J. Am. Ceram. Soc. 98, 1812–1817 (2015)

    Article  Google Scholar 

  14. C.J. Huang, K. Li, S.Y. Wu, X.L. Zhu, X.M. Chen, Variation of ferroelectric hysteresis loop with temperature in (SrxBa1–x)Nb2O6 unfilled tungsten bronze ceramics. J. Materiom. 1, 146–152 (2015)

    Article  Google Scholar 

Download references

Acknowledgements

The authors convey special thankful to Mr. C. Lakshmi Narayana M.A., English (PhD), Assistant Professor, Sreenivasa Ramanujan Institute of Technology, Anantapur for English language editing services of the whole manuscript. Thanks to Prof. T. Subbarao, Dept. of Physics, SK University, Anantapur for providing microwave heating facility.

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Correspondence to R. Padma Suvarna or K. Chandra Babu Naidu.

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Suresh Kumar, N., Padma Suvarna, R. & Chandra Babu Naidu, K. Structural and ferroelectric properties of microwave heated lead cobalt titanate nanoparticles synthesized by sol–gel technique. J Mater Sci: Mater Electron 29, 4738–4742 (2018). https://doi.org/10.1007/s10854-017-8429-6

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  • DOI: https://doi.org/10.1007/s10854-017-8429-6

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