Abstract
WO3 nanoparticle and flower-like WO3/graphene nanocomposite were successfully synthesized via a microwave-assisted hydrothermal method. The obtained samples were characterized by X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy and scanning electron microscope techniques. The gas-sensing performance of the as-synthesized materials was also investigated. The experimental results revealed that the graphene plays an important role in the crystal structure evolution from WO3 nanoparticle to flower-like WO3/graphene nanocomposite. The flower-like WO3/graphene nanocomposite shows far better gas-sensing properties for aniline gas at 80 °C.
Similar content being viewed by others
References
T. Li, W. Zeng, B. Miao, S. Zhao, Y. Li, H. Zhang, Mater. Lett. 144, 106–109 (2015)
M. Yu, H. Sun, X. Sun, F. Lu, T. Hu, G. Wang et al., Mater. Lett. 108, 29–32 (2013)
F. Liu, J.G. Kim, C.W. Lee, J.S. Im, Appl. Surf. Sci. 316, 604–609 (2014)
L. Wang, L. Yuan, X. Wu, J. Wu, C. Hou, S. Feng, RSC Adv. 4, 47670–47676 (2014)
C. Song, C. Li, Y. Yin, J. Xiao, X. Zhang, M. Song et al., Vacuum 114, 13–16 (2015)
S. Choi, A. Katoch, J. Kim, S. Kim, J. Mater. Chem. C 3, 1521–1527 (2015)
C. Wang, X. Li, C. Feng, Y. Sun, G. Lu, Sens. Actuators B 210, 75–81 (2015)
C. Feng, X. Li, J. Ma, Y. Sun, C. Wang, P. Sun, J. Zheng, G. Lu, Sens. Actuators B 209, 622–629 (2015)
Z. Cyrus, C. Olga, A. Teresa, R.M. Joan, R.R. Albert, Sens. Actuators B 140, 557–562 (2009)
X. Chu, T. Hu, F. Gao, Y. Dong, W. Sun, L. Bai, Mater. Sci. Eng. B 193, 97–104 (2015)
W. Zhou, F. Zhang, S. Liu, J. Wang, X. Du, D. Yin, L. Wang, RSC Adv. 4, 51362–51365 (2014)
H. Ying, Z.Y. Wang, Z.D. Guo, Z.J. Shi, S.F. Yang, Acta Phys. Chim. Sin. 27, 1482–1486 (2011)
Y.H. Gui, S.M. Li, J.Q. Xu, C. Li, Microelectron. J. 39, 1120–1125 (2008)
P.L. Gouma, K. Kalyanasundaram, J. Mater. Sci. 50, 3517–3522 (2015)
C. Wang, R. Sun, X. Li, Y. Sun, P. Sun, F. Liu, G. Lu, Sens. Actuators B 204, 224–230 (2014)
J. Guo, Y. Li, S. Zhu, Z. Chen, Q. Liu, D. Zhang et al., RSC Adv. 2(4), 1356–1363 (2012)
H. Huang, Z. Yue, G. Li, X. Wang, J. Huang, Y. Du et al., J. Mater. Chem. A1, 15110–15116 (2013)
D.Y. Lu, J. Chen, H.J. Chen, L. Gong, S.Z. Deng, N.S. Xu et al., Appl. Phys. Lett. 90, 041919/1–041919/3 (2007)
J. Guo, Y. Li, S. Zhu, Z. Chen, Q. Liu, D. Zhang et al., RSC Adv. 2(4), 1356–1363 (2012)
S. Srivastava, K. Jain, V.N. Singh, S. Singh, N. Vijayan, N. Dilawar et al., Nanotechnology 23(20), 205501/1–205501/7 (2012)
W. Zeng, H. Zhang, Z. Wang, Appl. Surf. Sci. 347, 73–78 (2015)
S. Choi, F. Fuchs, R. Demadrille, B. Grévin, B. Jang, S. Lee et al., Appl. Mater. Interfaces 6, 9061–9070 (2014)
Acknowledgments
The authors are very grateful for the support of the National Natural Science Foundation of China (Grant No. 21371158), the Foundation for University Key Teacher of Henan Province (Grant No. 122300410299), and the Program for Science and Technology of Zhengzhou (Grant No. 121PPTGG362-3).
Author information
Authors and Affiliations
Corresponding authors
Rights and permissions
About this article
Cite this article
Gui, Y., Liu, Z., Fang, S. et al. Synthesis of flower-like WO3/graphene nanocomposite by microwave-assisted hydrothermal method and the enhanced gas-sensing properties to aniline. J Mater Sci: Mater Electron 27, 2890–2895 (2016). https://doi.org/10.1007/s10854-015-4106-9
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10854-015-4106-9