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Optimization of the electrodeposition of Raney nickel on titanium substrate

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Abstract

The electrodeposition of Raney nickel onto a titanium grid substrate was investigated. Optimization of current density and charge density was performed via a factorial design experimental method to maximize the percentage of Raney nickel powder deposited on the grid. A scale-up of the deposition process was performed to demonstrate the feasibility of the procedure using larger substrates. Reproducible electrodes were obtained which can find applications in fuel cells as well as electrolytic hydrogen generators.

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Acknowledgements

The authors would like to acknowledge financial support from Ohio University: the Office of the Vice-President for Research, the Ohio University Foundation, the Department of Chemical Engineering, and the Stocker Research Fellowship.

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Correspondence to Gerardine G. Botte.

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A revised technical paper submitted to Journal of Materials Science for consideration for publication

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Cooper, M., Botte, G.G. Optimization of the electrodeposition of Raney nickel on titanium substrate. J Mater Sci 41, 5608–5612 (2006). https://doi.org/10.1007/s10853-006-0317-z

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  • DOI: https://doi.org/10.1007/s10853-006-0317-z

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