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Preparation and Application of Needle Extraction Device Packed with Sol–gel-Derived Perhydroxy Cucurbit[6]uril Coating Fiber

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Abstract

A novel needle extraction device packed with heat-resistant fibers coated with perhydroxy cucurbit[6]uril by sol–gel technology was first developed for the analysis of polycyclic aromatic hydrocarbons in actual water samples. Its performance was tested via purge and trap microextraction coupled with gas chromatography. The strong adsorption affinity between polycyclic aromatic hydrocarbons and (OH)12Q[6] was attributed to C–H···π interactions and π–π interactions. The parameters of the extraction device, such as extraction volume, extraction temperature, desorption time, ionic strength, and fiber number, were optimized. Under optimized conditions, the as-prepared extraction device showed good linearity within 0.5–1,500 µg L−1 with low detection limits (0.03–0.2 µg L−1). Moreover, the durability of the needle extraction device was excellent and can be used for 60 cycles. Furthermore, the loss rates of the coating fiber were less than 10% after storage for 3 days at room temperature, and the RSD was less than 6.4%.

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Acknowledgements

This work was supported by the National Natural Science Foundation of China (Grant numbers 21375046, 21605056), the Project of Science and Technology Development of Jilin Province (Grant number 20140203013GX), and the Natural Science Foundation of Jilin Province (Grant number 20180101292JC). The financial support from the Key Laboratory of Fine Chemicals of Jilin Province is also acknowledged.

Funding

This study was supported by the National Natural Science Foundation of China (Grant numbers 21375046, 21605056), the Project of Science and Technology Development of Jilin Province (Grant number 20140203013GX), and the Natural Science Foundation of Jilin Province (Grant number 20180101292JC). The financial support from the Key Laboratory of Fine Chemicals of Jilin Province is also acknowledged.

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Authors and Affiliations

  1. Department of Analytical Chemistry, Jilin Institute of Chemical Technology, 45 Chengde Street, Jilin, 132022, People’s Republic of China

    Xiaoyu Zhang, Jie Chen, Lili Lian, Xiyue Wang, Xiaoyang Guo, Huijun Chen, Bo Zhu, Shuang Hou & Dawei Lou

  2. Department of Analytical Chemistry, Jilin University, 2699 Qianjin Street, Changchun, 130012, People’s Republic of China

    Xiaoyu Zhang & Huijun Chen

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  1. Xiaoyu Zhang
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  2. Jie Chen
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  3. Lili Lian
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  4. Xiyue Wang
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  6. Huijun Chen
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  7. Bo Zhu
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  9. Dawei Lou
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Correspondence to Dawei Lou.

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Zhang, X., Chen, J., Lian, L. et al. Preparation and Application of Needle Extraction Device Packed with Sol–gel-Derived Perhydroxy Cucurbit[6]uril Coating Fiber. Chromatographia 82, 953–960 (2019). https://doi.org/10.1007/s10337-019-03720-1

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