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Experimental research on the influence of loading rate on the mechanical properties of limestone in a high-temperature state

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Abstract

Engineering problems associated with high-temperature rock, such as the deep disposal of high-level radioactive nuclear waste, underground gasification and storage of coal, development of geothermal resources, restoration of important buildings after a fire, among others, have drawn the interest of many engineers and become a new and developing field of rock mechanics. In our study, we conducted the uniaxial compression test under conditions of high temperatures (T) that range from 20 °C to 800 °C and loading rates (lr) that vary from 0.001 to 0.1 mm/s, using the MTS 816 rock mechanics testing system, with the aim to investigate the evolution of deformation and intensity parameters of the limestone. The results show that the uniaxial compression process of limestone at different temperatures and loading rates comprises four stages: compaction, flexibility, yielding and post-peak failure. With increasing temperature, the ductility of limestone, the peak strain and the maximum strain after failure increase, and the post-peak softening characteristics of limestone gradually become obvious; however, the peak stress and elastic modulus of limestone decrease gradually. With increasing loading rate, the slope of the stress–strain curve in the elastic stage increases, and the deformation and intensity parameters of limestone increase accordingly. At T ≤ 500 °C and lr ≤ 0.01 mm/s, the rock specimens undergo failure or tension–shear mixed failure. At T > 500 °C and lr > 0.01 mm/s, Y-shaped shear failure occurs in the rock specimens. The failure degree of the limestone becomes more severe with increasing temperature and loading rate. The results of this study provide a scientific basis for high-temperature rock engineering studies on the design and construction of deep geological underground storage areas for high-level radioactive nuclear wastes, geothermal development, among others.

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References

  • Bieniawski ZT (1970) Time-dependent behaviour of fractured rock. Rock Mech 2(3):123–137

    Article  Google Scholar 

  • Blanton TL (1981) Effect of strain rates from 10−2 to 10 sec−1 in triaxial compression tests on three rocks. Int J Rock Mech Min Geomech Abstr 18(1):47–62

    Article  Google Scholar 

  • Cai M, Kaiser PK, Suorineni F, Su K (2007) A study on the dynamic behavior of the Meuse/Haute-Marne argillite. Phys Chem Earth 32(8):907–916

    Article  Google Scholar 

  • Cho SH, Ogata YJ, Kaneko K (2003) Strain-rate dependency of the dynamic tensile strength of rock. Int J Rock Mech Min 40(5):763–777

    Article  Google Scholar 

  • Chong KP, Borest AP (1990) Strain rate dependent mechanical properties of New Albany reference shale. Int J Rock Mech Min Sci Geomech Abstr 27(3):199–205

    Article  Google Scholar 

  • Chopra PN (1997) High-temperature transient creep in olivine rocks. Tectonophysics 279(1–4):93–111

    Article  Google Scholar 

  • David C, Menéndez B, Darot M (1999) Influence of stress-induced and thermal cracking on physical properties and microstructure of La Peyratte granite. Int J Rock Mech Min 36(4):433–448

    Article  Google Scholar 

  • Duclos R, Paquet J (1991) High-temperature behaviour of basalt-role of temperature and strain rate on compressive strength and K 1C toughness of partially glassy basalts at atmospheric pressure. Int J Rock Mech Min Sci Geomech Abstr 28(1):71–76

    Article  Google Scholar 

  • Ferrero AM, Marini P (2001) Experimental studies on the mechanical behaviour of two thermal cracked marbles. Rock Mech Rock Eng 34(1):57–66

    Article  Google Scholar 

  • Glover PWJ, Baud P, Darot M, Meredith PG, Boon SA, LeRevelec M, Zoussi S, Reuschlé T (1995) α/β phase transition in quartz monitored using acousticemissions. Geophys J Int 120(3):775–782

    Article  Google Scholar 

  • Hajpál M (2002) Changes in limestone of historical monuments exposed to fire or high temperature. Fire Technol 38(4):373–382

    Article  Google Scholar 

  • Heuze FE (1983) High-temperature mechanical, physical and thermal properties of granitic rocks—a review. Int J Rock Mech Min Sci Geomech Abstr 20(1):3–10

    Article  Google Scholar 

  • Kilic O (2006) The influence of high temperatures on limestone p-wave velocity and schmidt hammer strength. Int J Rock Mech Min Sci 43(6):980–986

    Article  Google Scholar 

  • Leiss B, Molli G (2003) High-temperature’ texture in naturally deformed Carrara marble from the Alpi Apuane, Italy. J Struct Geol 25(4):649–658

    Article  Google Scholar 

  • Liu RC, Jiang YJ, Li B, Wang XS (2015) A fractal model for characterizing fluid flow in fractured rock masses based on randomly distributed rock fracture networks. Comput Geotech 65:45–55

    Article  Google Scholar 

  • Luo JA, Wang LG (2011) High-temperature mechanical properties of mudstone in the process of underground coal gasification. Rock Mech Rock Eng 44(6):749–754

    Article  Google Scholar 

  • Mahmutoglu Y (2006) The effects of strain rate and saturation on a micro-cracked marble. Eng Geol 82(3):137–144

    Article  Google Scholar 

  • Mao RR, Mao XB, Zhang LY, Liu RX (2015) Effect of loading rates on thecharacteristics of thermal damage for mudstone under different temperatures. Int J Min Sci Technol 25(5):797–801

    Article  Google Scholar 

  • Meng QB, Zhang MW, Han LJ, Pu H, Li H (2016) Effects of size and strain rate on the mechanical behaviors of rock specimens under uniaxial compression. Arab J Geosci 9:527–541

    Article  Google Scholar 

  • Okubo S, Nishimatsu Y, He C (1990) Loading rate dependence of class II rock behaviour in uniaxial and triaxial compression tests-an application of a proposed new control method. Int J Rock Mech Min Sci Geomech Abstr 27(6):559–562

    Article  Google Scholar 

  • Olsson WA (1991) The compressive strength of tuff as a function of strain rate from 10−6 to 103 sec. Int J Rock Mech Min Sci Geomech Abstr 28(1):115–118

    Article  Google Scholar 

  • Peng SS (1973) Time-dependent aspects of rock behavior as measured by a servocontrolled hydraulic testing machine. Int J Rock Mech Min Sci Geomech Abstr 10(3):235–246

    Article  Google Scholar 

  • Peng SS, Podnieks ER (1972) Relaxation and the behavior of failed rock. Int J Rock Mech Min Sci Geomech Abstr 9(2):699–700

    Article  Google Scholar 

  • Qi CZ, Wang MY, Qian QH (2009) Strain rate effects on the strength and fragmentation size of rocks. Int J Impact Eng 36(12):1355–1364

    Article  Google Scholar 

  • Ranjith PG, Viete DR, Chen BJ, Perera MSA (2012) Transformation plasticityand the effect of temperature on the mechanical behavior of Hawkesbury sandstone at atmospheric pressure. Eng Geol 151:120–127

    Article  Google Scholar 

  • Rocchi V, Sammonds PR, Kilburn CRJ (2004) Fracturing of etnean and vesuvian rocks at high temperatures and low pressures. J Volcanol Geotherm Res 132(2–3):137–157

    Article  Google Scholar 

  • Su HJ, Jing HW, Mao XB, Zhao HH, Yin Q, Wang C (2015) Size effect of sandstone after high temperature under uniaxial compression. J Cent South Univ 22(5):1901–1908

    Article  Google Scholar 

  • Sun Q, Zhang WQ, Xue L, Zhang Z, Su T (2015) Thermal damage pattern and thresholds of granite. Environ Earth Sci 74(3):2341–2349

    Article  Google Scholar 

  • Sun Q, Zhang WQ, Su T (2016) Variation of wave velocity and porosity of sandstone after high temperature heating. Acta Geophys 64(3):633–648

    Article  Google Scholar 

  • Tarasov BG (1990) Simplified method for determining the extent to which strain rate affects the strength and energy capacity of rock fracture. J Min Sci 26(4):315–320

    Google Scholar 

  • Tullis J, Yund RA (2012) Experimental deformation of dry westerly granite. J Geophys Res 82(36):5705–5718

    Article  Google Scholar 

  • Xu XL, Zhang ZZ (2016) Fractal characteristics of rock fracture surface under triaxial compression after high temperature. Adv Mater Sci Eng 9:1–10

    Google Scholar 

  • Xu XL, Gao F, Shen XM, Xie HP (2008) Mechanical characteristics and microcosmic mechanisms of granite under temperature loads. J China U Min Techno 18(3):413–417

    Article  Google Scholar 

  • Yang SQ, Jing HW, Huang YH, Ranjith PG, Jiao YY (2014) Fracture mechanical behavior of red sandstone containing a single fissure and two parallel fissures after exposure to different high temperature treatments. J Struct Geol 69(Part A):245–264

    Article  Google Scholar 

  • Yang SQ, Ranjith PG, Jing HW, Tian WL, Ju Y (2017) An experimental investigation on thermal damage and failure mechanical behavior of granite after exposure to different high temperature treatments. Geothermics 65:180–197

    Article  Google Scholar 

  • Zhang QB, Zhao J (2014) A review of dynamic experimental techniques and mechanical behaviour of rock materials. Rock Mech Rock Eng 47(4):1411–1478

    Article  Google Scholar 

  • Zhang ZX, Yu J, Kou SQ, Lindqvist PA (2001) Effects of high temperature on dynamic rock fracture. Int J Rock Mech Min Sci 38(2):211–225

    Article  Google Scholar 

  • Zhang LY, Mao XB, Lu AH (2009) Experimental study on the mechanical properties of rocks at high temperature. Sci China Technol Sc 52(3):641–646

    Article  Google Scholar 

  • Zhao YS, Wan ZJ, Feng ZJ, Yang D, Zhang Y, Qu F (2012) Triaxial compression system for rock testing under high temperature and high pressure. Int J Rock Mech Min 52:132–138

    Article  Google Scholar 

Download references

Acknowledgements

The financial and general support for this research as provided by the National Key R&D Program of China (No. 2016YFC0600900), National Natural Science Foundation of China (Nos. 51504237, 51704280, 51734009) and China Postdoctoral Science Foundation (No. 2017 T100420) is gratefully acknowledged.

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Correspondence to Mingwei Zhang.

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Meng, Q., Zhang, M., Han, L. et al. Experimental research on the influence of loading rate on the mechanical properties of limestone in a high-temperature state. Bull Eng Geol Environ 78, 3479–3492 (2019). https://doi.org/10.1007/s10064-018-1332-4

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  • DOI: https://doi.org/10.1007/s10064-018-1332-4

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