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Monophthalates with Oxidized C5-Carbon in the Ester Chain: A Simple Synthetic Access to Two Major Metabolites of Bis-(2-ethylhexyl)-phthalate

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Summary.

 The synthesis of two oxidized metabolites of bis-(2-ethylhexyl)-phthalate is described. The target structures were obtained by esterification of the appropriate alcohol carrying a protected hydroxy group with phthalic anhydride, followed by deprotection and further oxidation.

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Authors and Affiliations

  1.  Institut für Dünnschichttechnologie und Mikrosensorik, D-14513 Teltow, Germany, , , , , , DE

    Hans-Detlev Gilsing & Dietrich Prescher

  2.  Institut und Poliklinik für Arbeits-, Sozial- und Umweltmedizin der Universität Erlangen-Nürnberg, D-91054 Erlangen, Germany, , , , , , DE

    Jürgen Angerer

Authors
  1. Hans-Detlev Gilsing
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  2. Jürgen Angerer
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  3. Dietrich Prescher
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Received February 26, 2002. Accepted March 6, 2002

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Gilsing, HD., Angerer, J. & Prescher, D. Monophthalates with Oxidized C5-Carbon in the Ester Chain: A Simple Synthetic Access to Two Major Metabolites of Bis-(2-ethylhexyl)-phthalate. Monatshefte fuer Chemie 133, 1147–1155 (2002). https://doi.org/10.1007/s007060200084

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  • DOI: https://doi.org/10.1007/s007060200084

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