Skip to main content
SpringerLink
Log in

A one-pot synthesis of N-alkylthiazoline-2-thiones from CS2, primary amines, and 2-chloro-1,3-dicarbonyl compounds in water

  • Original Paper
  • Published:
Monatshefte für Chemie - Chemical Monthly Aims and scope Submit manuscript

Abstract

A simple synthesis of N-alkylthiazoline-2-thiones by reaction of primary amines, carbon disulfide, and 2-chloro-1,3-dicarbonyl compounds in water is described. Proceeding without catalyst under one-pot conditions in high yields and with broad scope, this method high synthetic utility.

Graphical abstract

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Scheme 1
Scheme 2

Similar content being viewed by others

References

  1. Cristiani F, Devillanova FA, Verani G (1982) Mol Spectrosc 38:1299

    Google Scholar 

  2. Cox PJ, Aslanidis P, Karagiannidis P, Hadjikakou S (2000) Inorg Chim Acta 310:268

    Article  CAS  Google Scholar 

  3. Toplak RB, Rocherulle P, Lorcy D (2002) Tetrahedron Lett 43:3879

    Article  CAS  Google Scholar 

  4. Eid S, Guerro M, Lorcy D (2006) Tetrahedron Lett 47:8333

    Article  CAS  Google Scholar 

  5. Hirano S, Takagi Y (1984) US Patent 4,429,036, Chem Abstr 99:46004b

  6. Humphlett WJ, Lamon RW (1963) J Org Chem 29:2146

    Article  Google Scholar 

  7. Humphlett WJ, Lamon RW (1963) J Org Chem 29:2148

    Article  Google Scholar 

  8. Lamon RW, Humphlett WJ (1967) J Heterocycl Chem 4:605

    Article  CAS  Google Scholar 

  9. Dunn AD, Rudorf W (1989) Carbon disulphide in organic chemistry. Wiley, New York, pp 226–315

    Google Scholar 

  10. Ze-Mei G, Qin L, Shao-Jun Z, Tie-Ming C, Yu-Xin C, Run-Tao L (2006) Chin J Chem 24:381

    Article  Google Scholar 

  11. Yavari I, Hajinasiri R, Sayyed-Alangi SZ, Iravani N (2008) Monatsh Chem 139:1029

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Chemistry Department, Tarbiat Modares University, P.O. Box 14115-175, Tehran, Iran

    Issa Yavari, Mehdi Sirouspour & Sanaz Souri

Authors
  1. Issa Yavari
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Mehdi Sirouspour
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Sanaz Souri
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Issa Yavari.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Yavari, I., Sirouspour, M. & Souri, S. A one-pot synthesis of N-alkylthiazoline-2-thiones from CS2, primary amines, and 2-chloro-1,3-dicarbonyl compounds in water. Monatsh Chem 141, 49–52 (2010). https://doi.org/10.1007/s00706-009-0227-2

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00706-009-0227-2

Keywords

Search

Navigation