Abstract.
The application of ESEM technology to the conservation of cultural heritage and other fields is reviewed. Several applications are presented with a focus on reaction kinetics and micro to nano-scale material behaviours, including time-lapse studies of reaction kinetics for NaCl and NaNO3; verification of the stone decay mechanism at the site of Copan, Honduras; and ESEM/EDS analysis of the first photograph (1826). A review of other ESEM applications reveals some important trends, especially in the materials science, electronics and biosciences fields, such as quantitative ESEM/EDS; 1.8 nm resolution imaging of extreme insulators in VP/ESEM; and ESEM analysis of emulsions and cells.
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References
A L Fletcher B L Thiel A M Donald (1999) J Microscopy 196 26 Occurrence Handle10.1046/j.1365-2818.1999.00590.x
E Doehne (1998) Microscop Microanal 4 IssueID2 292
G R Watt B J Griffin P D Kinny (2000) Am Mineral 85 IssueID11–12 1784 Occurrence Handle1:CAS:528:DC%2BD3cXotV2nurw%3D
E Doehne D C Stulik (1990) Scanning Microscopy 4 IssueID2 275 Occurrence Handle1:CAS:528:DyaK3cXlslWjsbY%3D
K C A Smith C W Oatley (1955) Br J Appl Phys 6 391 Occurrence Handle10.1088/0508-3443/6/11/304
von Ardenne M (1985) On the history of scanning electron microscopy, of the electron microprobe, and of early contributions to transmission electron microscopy. The beginnings of electron microscopy. In: Hawkes P (ed). pp 1–21
M von Ardenne (1940) Elektronen-Übermikroskopie Springer Berlin
G D Danilatos V N E Robinson (1979) Scanning 2 72
D A Moncrieff P R Barker V N E Robinson (1979) J Phys D Appl Phys 12 481 Occurrence Handle1:CAS:528:DyaE1MXhsF2ktLo%3D Occurrence Handle10.1088/0022-3727/12/4/005
V N E Robinson (1975) J Microscopy 103 IssueID1 71 Occurrence Handle1:STN:280:DyaE2M7pt1Shsw%3D%3D
G D Danilatos (1990) Scanning 12 IssueID1 23
G D Danilatos (1990) Adv Electronic Electron Phys 78 102
Danilatos G D (1990) Detection by induction in the environmental SEM. In XIIth International Conference Electron Microscopy. San Francisco Press, San Francisco
G D Danilatos (1990) J Microscopy 160 IssueID1 9
G D Danilatos (1990) Scanning Microscopy 4 IssueID4 799
Peters K R (1992) Principles of low vacuum scanning electron microscopy. 50th Annual Meeting of the Electron Microscopy Society of America. San Francisco Press, San Francisco
Doehne E, Stulik D (1991) Mat Res Soc, 9800 McKnight Rd., Suite 327, Pittsburgh, pp 31–38
Anon (1999) ArticleTitleFirst roadmap workshop for environmental scanning electron microscopy J Res Nat Inst Standards Technol 104 IssueID3 310
E M Griffith G D Danilatos (1993) Microscop Res Technique 25 IssueID5–6 353 Occurrence Handle10.1002/jemt.1070250502
Doehne E (1997) ESEM development and application in cultural heritage conservation. In-situ microscopy in materials research. In: Gai P (ed). Kluwer Academic Publishers, Dordrecht, pp 45–62
C Rodriguez-Navarro E Doehne (1999) Am Lab 31 IssueID10 28
G D Danilatos R Postale (1982) Scan Electron Micros 1982 1
FEI (2005) FEI Introduces Nova NanoSEM. nanotechwire.com
R A Carlton C E Lyman J E Roberts (2004) Microscop Microanal 10 IssueID6 753 Occurrence Handle1:CAS:528:DC%2BD2cXhtVSgur%2FK
R A Carlton C E Lyman J E Roberts (2004) Scanning 26 167 Occurrence Handle10.1002/sca.4950260404
M P Rossi et al. (2004) Nano Lett 4 IssueID5 989 Occurrence Handle1:CAS:528:DC%2BD2cXjtVCjtbY%3D Occurrence Handle10.1021/nl049688u
D J Stokes B L Thiel A M Donald (2000) Scanning 22 IssueID6 357 Occurrence Handle1:CAS:528:DC%2BD3MXhtleruw%3D%3D Occurrence Handle10.1002/sca.4950220604
R G Mathews A M Donald (2002) Scanning 24 IssueID2 75 Occurrence Handle1:CAS:528:DC%2BD38XjtlCnsrc%3D Occurrence Handle10.1002/sca.4950240205
K J McKinlay et al. (2004) J Biomed Mat Res Part A 69A IssueID2 359 Occurrence Handle1:CAS:528:DC%2BD2cXjsVGqt7o%3D Occurrence Handle10.1002/jbm.a.30011
Stokes D J et al (2002) Characterization of biomedical materials, cells & interfaces using Environmental SEM (ESEM). Materials Research Society Symposium Proceedings, 2002. 711 (Advanced Biomaterials: Characterization, Tissue Engineering and Complexity) pp 113–118
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Doehne, E. ESEM Applications: From Cultural Heritage Conservation to Nano-Behaviour. Microchim Acta 155, 45–50 (2006). https://doi.org/10.1007/s00604-006-0505-1
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DOI: https://doi.org/10.1007/s00604-006-0505-1