Abstract
The coalfield fire is determined by fractures of coal and rock that provide tunnel for gases and heat exchange. To study fracture propagation at high temperatures, high-resolution X-ray computed tomography (CT) was used to scan anthracite and mudstone samples collected from the Qinshui coalfield, Shanxi Province, northern China. The samples were scanned at 100 °C intervals as they were subjected to temperatures of up to 500 °C. Three-dimensional images were reconstructed by the CT software to analyze changes in the fractures and pores in the samples. The experimental results show that fracturing of anthracite began at 200 °C. The generation rate of fractures in the coal samples increases slowly below 300 °C, but above 300 °C there is a sharp increase in fracture development. This indicates that the thermal fracturing temperature threshold for anthracite is 300 °C. During the experiment, it was found that preexisting fractures, voids, and regenerative fractures formed around the hard portions of anthracite particles or along the weak boundaries between particles. Some regenerative fractures developed along the fabric of the relatively crystalline particles within the particle and terminate at the edge of the particle or where the fracture encounters a harder portion of coal. Some fractures even expanded enough to be transformed into voids as temperatures rose. In the mudstone, the porosity changed suddenly at 300 °C. This indicated that there was a void generated at 200 °C, but the void expanded when the temperature was increased. However, changes in the void were not obvious from 200 to 300 °C.
Similar content being viewed by others
References
Anusavice KJ, Hojjatie B (1991) Effect of thermal tempering on strength and crack propagation behavior of feldspathic porcelains. J Dent Res 70(6):1009–1013
Cai YD, Liu DM, Mathews JP, Pan ZJ, Elsworth D, Yao YB, Li JQ, Guo XQ (2014) Permeability evolution in fractured coal-combining triaxial confinement with X-ray computed tomography, acoustic emission and ultrasonic techniques. Int J Coal Geol 122:91–104
Dacombe P, Pourkashanian M, Williams A, Yap L (1999) Combustion-induced fragmentation behavior of isolated coal particles. Fuel 78:1847–1857
Dewanckele J, Kock TD, Boone MA, Cnudde V, Brabant L, Boone MN, Fronteau G, Hoorebeke LV, Jacobs P (2012) 4D imaging and quantification of pore structure modifications inside natural building stones by means of high resolution X-ray CT. Sci Total Environ 416:436–448
Dwivedi RD, Goel RK, Prasad VVR, Sinha A (2008) Thermo-mechanical properties of Indian and other granites. Int J Rock Mech Min Sci 45:303–315
Gellert R, Rieder R, Anderson RC et al (2004) Chemistry of rocks and soils in gusev crater from the alpha particle X-ray spectrometer. Science 305:829–832
Golab A, Ward CR, Permana A, Lennox P, Botha P (2013) High-resolution three-dimensional imaging of coal using microfocus X-ray computed tomography, with special reference to modes of mineral occurrence. Int J Coal Geol 113:97–108
Heap MJ, Baud P, Meredith PG (2009) Influence of temperature on brittle creep in sandstone. Geophys Res Lett. doi:10.1029/2009GL039373
Heard HC (1980) Thermal expansion and inferred permeability of climax quartz monzonite to 300 °C and 27.6 MPa. Int J Rock Mech Min Sci Geomech Abstr 17:289–296
Holman JP (1994) Experimental methods for engineers, 6th edn. McGraw-Hill, New York
Homand-Etienne F, Houpert R (1989) Thermally induced micro cracking in granites: characterization and analysis. Int J Rock Mech Min Sci Geomech Abstr 26(2):125–134
ISO 11760 (2005) Classification of coals. International Organization for Standardization-ISO, Geneva, p 9
Kou SQ (1987) Effect of thermal cracking damage on the deformation and failure of granite. Acta Mech Sin 19(6):550–556
Kuenzer C, Zhang J, Sun Y, Jia Y, Dech S (2012) Coal fires revisited: the Wuda coal field in the aftermath of extensive coal fire research and accelerating extinguishing activities. Int J Coal Geol 102:75–86
Mao XB, Zhang LY, Li TZ, Liu HS (2009) Properties of failure mode and thermal damage for limestone at high temperature. Min Sci Technol 19:0290–0294
Mayo S, Josh M, Nesterets Y, Esteban L, Pervukhina M, Clennell MB, Maksimenko A, Hall C (2015) Quantitative micro-porosity characterization using synchrotron micro-CT and xenon K-edge subtraction in sandstones, carbonates, shales and coal. Fuel 154:167–173
Mazumder S, Wolf KHAA, Elewaut K, Ephraim R (2006) Application of X-ray computed tomography for analyzing cleat spacing and cleat aperture in coal samples. Int J Coal Geol 68:205–222
Meng QR, Zhao YS, Hu YQ, Feng ZC, Xu SG (2011) Micro-CT experimental of the thermal cracking of brown coal. J China Coal Soc 36(5):855–860 (in Chinese)
Ortega A, Rouquerol F, Akhouayri S, Laureiro Y, Rouquerol J (1993) Kinetical study of the thermolysis of kaolinite between −30 and 1000 °C by controlled rate evolved gas analysis. Appl Clay Sci 8:207–214
Paul S, Chatterjee R (2011) Mapping of cleats and fractures as an indicator of in situ stress orientation, Jharia coalfield, India. Int J Coal Geol 88(2):113–122
Rieder R, Gellert R, Anderson RC et al (2004) Chemistry of rocks and soils at meridiani planum from the alpha particle X-ray spectrometer. Science 306:1746–1749
Sheppard AP, Sok RM, Averdunk H (2004) Techniques for image enhancement and segmentation of tomographic images of porous materials. Phys A 339:145–151
Somerton WH, Gupta VS (1965) Role of fluxing agents in thermal alteration of sandstones. J Petrol Technol 17(5):585–588
Somerton WH, Mehta MM, Dean GW (1965) Thermal alteration of sandstones. J Petrol Technol 17(5):589–593
Van Geet M (2001) Optimization of microfocus X-ray computer tomography for geological research with special emphasis on coal components (macerals) and fractures (cleats) characterization. Ph.D. thesis, K. U. Leuven, Belgium
Vandersteen K, Busselen B, Abeele VD, Carmeliet J (2003) Quantitative characterization of fracture apertures using microfocus computed tomography. In: Mees F, Swennen R, Van Geet M, Jacobs P (eds) Applications of X-ray computed tomography in the geosciences. Geol Soc Spec Publ 215: 61–68
Varslot T, Kingston A, Myers G, Sheppard A (2011) High-resolution helical cone-beam micro-CT with theoretically-exact reconstruction from experimental data. Med Phys 38:5459–5476
Verhelst F, Vervoort A, De Bosscher P, Marchal G (1995) X-ray computerized tomography: determination of heterogeneities in rock samples. In: 8th ISRM congress, 25–29 September, Tokyo, Japan. (Doc ID: ISRM-8CONGRESS-1995-023)
Wang HP, Yang YS, Wang YD, Yang JL, Jia J, Nie YH (2013) Data-constrained modelling of an anthracite coal physical structure with multi-spectrum synchrotron X-ray CT. Fuel 106:219–225
Xiao Y (2013) Study on the mechanical characteristics of coal-rock mass of coalfield fires with thermo-hydro-mechanical coupling for fissure seepage. Ph.D. thesis. Xi’an University of Science and Technology, China (in Chinese)
Xie KC (2015) Structure and reactivity of coal. Springer, Heidelberg. doi:10.1007/978-3-662-47337-5
Xu XL (2008) Research on the mechanical characteristics and micromechanism of granite under temperature loads. Ph.D. thesis. China University of Mining and technology, China (in Chinese)
Xu XL, Gao F, Shen XM, Xie HP (2008) Mechanical characteristics and microcosmic mechanisms of granite under temperature loads. J China Univ Min Technol 18:0413–0417
Yang D, Kang ZQ, Zhao J, Zhao YS (2011) CT experiment research of oil shale under high temperature. J Taiyuan Univ Technol 42(3):255–257 (in Chinese)
Yu YM, Hu YQ, Liang WG, Meng QR, Feng ZC, Yu CT (2010) Micro-CT experimental research of lean coal thermal cracking laws. J China Coal Soc 35(10):1696–1700 (in Chinese)
Yu YM, Liang WG, Hu YQ, Meng QR (2012) Study of micro-pores development in lean coal with temperature. Int J Rock Mech Min Sci 51:91–96
Zhang LY, Mao XB, Lu AH (2009) Experimental study on the mechanical properties of rocks at high temperature. Sci China Ser E Tech Sci 52(3):641–646
Zhao YS, Meng QR, Kang TH, Zhang N, Xi BP (2008) Micro-CT experimental technology and meso-investigation on thermal fracturing characteristics of granite. Chin J Rock Mech Eng 27(1):28–34 (in Chinese)
Zuo JP, Xie HP, Zhou HW, Peng SP (2007) Experimental research on thermal cracking of sandstone under different temperature. Chin J Geophys 50(4):1150–1155 (in Chinese)
Acknowledgments
The authors gratefully acknowledge Professors Alexandra Golab and Colin R. Ward (University of New South Wales, Australia), who provided much assistance with the CT images reconstruction. This work was supported by the National Natural Science Foundation of China (Nos. 51204136, 51504187), and the Industrial Science and Technology Project of Shaanxi Province (No. 2016GY-192).
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Xiao, Y., Lu, JH., Wang, CP. et al. Experimental Study of High-Temperature Fracture Propagation in Anthracite and Destruction of Mudstone from Coalfield Using High-Resolution Microfocus X-ray Computed Tomography. Rock Mech Rock Eng 49, 3723–3734 (2016). https://doi.org/10.1007/s00603-016-1006-0
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s00603-016-1006-0