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Synthesis, characterization, and thermal properties of biodegradable polyetheresteramide copolymers based on 11-aminoundecanoic acid

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Abstract

In this work, new aliphatic polyetheresteramide copolymers based on ε-caprolactone, 11-aminoundecanoic acid, and poly(ethylene glycol) (PEG) were synthesized by the melt polycondensation method. The copolymers obtained were characterized by 1H NMR, differential scanning calorimetry, thermogravimetric analysis/differential thermogravimetry, and wide-angle X-ray diffraction. Water absorption and hydrolytic degradation behavior was also studied. With the increase in PEG content, water absorption and the hydrolytic degradation rate increased accordingly.

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Acknowledgements

This work was sponsored by the "Outstanding young scientist fund of Sichuan province" and the "Hundreds of talents program" of the Chinese Academy of Sciences.

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Authors and Affiliations

  1. Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, 610041, Chengdu, China

    Z. Y. Qian, S. Li, Y. He, H. L. Zhang & X. B. Liu

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  1. Z. Y. Qian
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  2. S. Li
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  3. Y. He
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  4. H. L. Zhang
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  5. X. B. Liu
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Correspondence to X. B. Liu.

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Qian, Z.Y., Li, S., He, Y. et al. Synthesis, characterization, and thermal properties of biodegradable polyetheresteramide copolymers based on 11-aminoundecanoic acid. Colloid Polym Sci 282, 133–140 (2003). https://doi.org/10.1007/s00396-003-0910-5

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  • DOI: https://doi.org/10.1007/s00396-003-0910-5

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