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Improvements of a combined size exclusion chromatography and solid phase extraction approach for the clean-up of marine sediment samples for trace analysis of pesticides

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Abstract

 Two methods based on gel permeation chromatography (GPC) [size exclusion chromatography] for the analysis of traces (ng/kg) of nitrogen and phosphorus containing pesticides (like triazines or phosphothionates) from marine sediment samples are compared: A macro GPC with Biobeads SX-3 and a chromatography on a high-performance (HP-GPC) column with UV-detection. Results for eight triazine herbicides, two triazine metabolites, the phenylurea derivative linuron, two acetanilides and two organophosphorus compounds are given. Concentrations obtained with the HP-GPC are compared with those obtained with a macro GPC approach in an earlier study.

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Received: 4 October 1996/Revised: 20 December 1996/Accepted: 24 December 1996

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Bester, K., Hühnerfuss, H. Improvements of a combined size exclusion chromatography and solid phase extraction approach for the clean-up of marine sediment samples for trace analysis of pesticides. Fresenius J Anal Chem 358, 630–634 (1997). https://doi.org/10.1007/s002160050481

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  • DOI: https://doi.org/10.1007/s002160050481

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