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SPME in environmental analysis

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Abstract

Recent advances in the use of solid-phase microextraction (SPME) in environmental analysis, including fiber coatings, derivatization techniques, and in-tube SPME, are reviewed in this article. Several calibration methods for SPME, including traditional calibration methods, the equilibrium extraction method, the exhaustive extraction method, and several diffusion-based calibration methods, are presented. Recent developed SPME devices for on-site sampling and several applications of SPME in environmental analysis are also introduced.

 

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Abbreviations

AED:

Atomic emission detection

BTEX:

Benzene, toluene, ethylbenzene, and xylenes

C[4]/OH-TSO:

25,27-Dihydroxy-26,28-oxy(2′,7′-dioxo-3′,6′-diazaoctyl)oxy-p-tert-butylcalix[4]arene/hydroxy-terminated silicon oil

CAR:

Carboxen

CW:

Carbowax

DBA:

Dibutylamine

DCP:

Dichloropropene

DELCD:

Dry electrolytic conductivity detector

DI:

Direct immersing

DVB:

Divinylbenzene

ECD:

Electron capture detector

FID:

Flame ionization detector

FLD:

Fluorescence detection

GC:

Gas chromatography

HPLC:

High-performance liquid chromatography

HS:

Headspace

IMS:

Ion mobility spectrometry

MCC:

Multi-capillary column

MEKC:

Micellar electrokinetic chromatography

MITC:

Methyl isothiocyanate

MS:

Mass spectrometer

MTBE:

Methyl tert-butyl ether

MTMOS:

Methyltrimethoxysilane

NIOSH:

The National Institute for Occupational Safety and Health

NPD:

Nitrogen/phosphorus detector

PA:

Polyacrylate

PAH:

Polycyclic aromatic hydrocarbon

PBDE:

Polybrominated diphenyl ether

PBB:

Polybrominated biphenyl

PBP:

Persistent and bioaccumulative pollutants

PCB:

Polychlorinated biphenyl

PCDD/F:

Polychlorinated dibenzodioxins/dibenzofurans

PDMS:

Polydimethylsiloxane

PEG:

Polyethylene glycol

PFBHA:

o-(2,3,4,5,6-pentafluorobenzyl) hydroxylamine hydrochloride

PFPD:

Pulsed flame photometric detector

PID:

Photoionization detector

PPY:

Polypyrrole

PPY-DS:

Dodecylsulfate-doped polypyrrole

PTMOS:

Phenyltrimethoxysilane

PVA:

Polyvinyl alcohol

SPE:

Solid-phase extraction

SPME:

Solid-phase microextraction

SVOC:

Semi-volatile organic compound

TDI:

Toluene diisocyanate

TNT:

2,4,6-Trinitrotoluene

TWA:

Time-weighted average

VOC:

Volatile organic compound

VSC:

Volatile sulfur compound

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Authors and Affiliations

  1. School of Chemistry and Chemical Engineering, Sun Yat-sen University, Guangzhou, 510275, People’s Republic of China

    Gangfeng Ouyang

  2. Department of Chemistry, University of Waterloo, Waterloo, ON, N2L 3G1, Canada

    Janusz Pawliszyn

Authors
  1. Gangfeng Ouyang
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  2. Janusz Pawliszyn
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Correspondence to Janusz Pawliszyn.

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Ouyang, G., Pawliszyn, J. SPME in environmental analysis. Anal Bioanal Chem 386, 1059–1073 (2006). https://doi.org/10.1007/s00216-006-0460-z

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  • DOI: https://doi.org/10.1007/s00216-006-0460-z

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