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Determination of residual pesticides in olive oil by GC–MS and HPLC–MS after extraction by size-exclusion chromatography

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Abstract

This work describes the development of a method for analyzing pesticide residues in olive oil by GC–MS and HPLC–MS. Pesticides were separated from the oily matrix by size-exclusion chromatography. After extraction, 20 pesticides were separated and analyzed by GC–MS and 11 others HPLC–MS in electrospray mode. The development of this method enabled us to identify and quantify the pesticides of interest.

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Authors and Affiliations

  1. Service Central d'Analyse, USR 059, CNRS, BP 22, 69390, Vernaison, France

    Sami Barrek, Olivier Paisse & Marie-Florence Grenier-Loustalot

Authors
  1. Sami Barrek
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  2. Olivier Paisse
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  3. Marie-Florence Grenier-Loustalot
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Correspondence to Marie-Florence Grenier-Loustalot.

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Barrek, S., Paisse, O. & Grenier-Loustalot, MF. Determination of residual pesticides in olive oil by GC–MS and HPLC–MS after extraction by size-exclusion chromatography. Anal Bioanal Chem 376, 355–359 (2003). https://doi.org/10.1007/s00216-003-1917-y

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  • DOI: https://doi.org/10.1007/s00216-003-1917-y

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