Abstract
Recent developments in sample rotation technology have had a profound impact on magic-angle-spinning NMR. First, rotation frequencies approaching, and even exceeding, strong homonuclear spin interactions have made high-resolution solid-state 1H spectroscopy much more accessible. Second, the new concept of fast rotation sweep spectroscopy has emerged. Third, high-resolution NMR at cryogenic temperatures has become feasible, offering an enormous sensitivity gain and the opportunity to study a wide range of physical phenomena.
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© 2005 Springer-Verlag Berlin Heidelberg
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Samoson, A., Tuherm, T., Past, J., Reinhold, A., Anupõld, T., Heinmaa, I. (2005). New Horizons for Magic-Angle Spinning NMR. In: Klinowski, J. (eds) New Techniques in Solid-State NMR. Topics in Current Chemistry, vol 246. Springer, Berlin, Heidelberg. https://doi.org/10.1007/b98647
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DOI: https://doi.org/10.1007/b98647
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Publisher Name: Springer, Berlin, Heidelberg
Print ISBN: 978-3-540-22168-5
Online ISBN: 978-3-540-31473-8
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