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Bestimmung von Zearalenon in Speiseölen mit GPC und LC-ESI-MS/MS

Determination of zearalenone in edible oils with SEC and LC-ESI-MS/MS

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Abstract

A new method for the determination of zearalenone in edible oils with size exclusion chromatography (SEC) followed by LC-MS/MS as well as HPLC-FLD was developed and validated. By using the LC-MS/MS determination no further clean up step is necessary after the SEC. The correlation coefficient of 0.999 for the two detection systems is acceptable. In this research 77 edible oils were analyzed. The mean average value of 38 corn germ oils was 169 μg/kg, the maximum value amounted up to 921 μg/kg.

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Authors and Affiliations

  1. Bundesinstitut für Risikobewertung, Thielallee 88-92, D-14195, Berlin

    O. Kappenstein, H. St. Klaffke, I. Mehlitz, R. Tiebach, R. Weber & R. Wittkowski

  2. Bayerische Landesanstalt für Landwirtschaft, Vöttinger Strasse 38, D-85354, Freising

    J. Lepschy

Authors
  1. O. Kappenstein
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  2. H. St. Klaffke
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  3. I. Mehlitz
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  4. R. Tiebach
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  5. R. Weber
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  6. J. Lepschy
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  7. R. Wittkowski
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Corresponding author

Correspondence to O. Kappenstein.

Additional information

Financial support: Bundesministerium für Verbraucherschutz, Emänrung und Landwirtschaft, Verbundforsonungsvorhaben, Vorkommen und Analytik von Fusarientoxinen (Deoxynivalenol und Zearalenon) sowle Aufranme dese. Toxine durch den deutschen Verpradcher.

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Kappenstein, O., Klaffke, H.S., Mehlitz, I. et al. Bestimmung von Zearalenon in Speiseölen mit GPC und LC-ESI-MS/MS. Mycotox Res 21, 3–6 (2005). https://doi.org/10.1007/BF02954804

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  • DOI: https://doi.org/10.1007/BF02954804

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