Abstract
The kinetics of the disappearance (spreading) of extrinsic grain boundary dislocations (EBGDs) at random grain boundaries has been investigated in a low-carbon austenitic stainless steel (0.01C-19Cr-18Ni) by measuring in TEM their disappearance times at the temperature range 360 to 450 °C. Experimental results fit most satisfactorily to a kinetic equation of the general form:t d =AT d exp(ΔH b /RT d ) derived by Johannesson and Thölen10 and Lojkowski and Grabskiii12 assuming either a dissociation into discrete structural grain boundary dislocation or the core spreading, respectively. Additional spreading experiments performed on commercial 316 austenitic stainless steel also support this general equation. Calculations employing experimental results indicate that the spreading time of a parallel component of the EGBD's Burgers vector is negligible and does not play any role during the process. Johannesson and Thölen10 and Lojkowski and Grabskiii12 models are practically indistinguishable assuming that in the J & T model an EGBD dissociates into an array of grain boundary dislocations with the magnitude of the Burgers vectorb b ≊ 0.07 nm. The TEM photographic documentation of the spreading clearly indicates that some grain boundaries exhibiting fine lines (not Moiré fringes) behave during spreading as random (general) boundaries. On the other hand, some grain boundaries free of any fine lines exhibit very high spreading temperature indicating a special behavior.
Similar content being viewed by others
References
Y. Ishida, T. Hasegawa, and F. Nagata:Trans. JIM, 1968, vol. 9 (Suppl.), pp. 504–08.
P. H. Pumphrey and H. Gleiter:Phil. Mag., 1974, vol 30, pp. 593–602.
P. H. Pumphrey:J. Physique, 1975, vol. 36 (Suppl to No 10) pp. C4 23–33.
PH. Pumphrey and H. Gleiter:Phil. Mag., 1975, vol 32, pp. 881–85.
R. A. Varin:Phys. Stat. Sol. (a), 1979, vol. 52, pp. 347–56.
R. A. Varin:J. Mater. Sci., 1979, vol. 14, pp. 811–16.
R.A. Varin, W. Lojkowski, and R.Z. Valiev:Scr. Metall., 1981, vol. 15, pp. 795–98.
R. A. Varin:Mater. Sci. Eng., 1984, vol. 66, pp. 97–105.
R.A. Varin:Phys. Stat. Sol. (a), 1982, vol. 73, pp. K51–55.
T. Johannesson and A. Thölen:Metal Sci. J., 1972, vol. 6, pp. 189–94.
W. Lojkowski: Ph.D. Thesis, The Warsaw Technical University, 1980.
W. Lojkowski and M. W. Grabski: in “Deformation of Polycrystals; Mechanisms and Microstructures,”Proc. 2nd Risø lnt. Symposium on Metallurgy and Materials Science, September 1981, N. Hansen, A. Horsewell, T. Leffers, and H. Lilholt, eds., Risø National Laboratory, Risø, 1981, pp. 329–34.
A. Thölen: inProc. Eighth Int. Congr. on EM, Canberra, 1974, vol. 1, pp. 606–07.
R.A. Varin:Z. Metallkde., 1982, vol. 73, pp. 654–58.
R.A. Varin and K. Tangri:Metall. Trans. A, 1981, vol. 12A, pp. 1859–66.
R. A. Varin and K. Tangri:Z. Metallkde., 1982, vol. 73, pp. 144–48.
R. V. Patil and B. D. Sharma:Met. Sci., 1982, vol. 16, pp. 389–92.
K.J. Kurzydlowski, R.A. Varin, and W. Zielinski:Acta Metall., 1984, vol. 32, pp. 71–78.
G. Wirmark, J.O. Nilsson, and G. L. Dunlop:Phil. Mag. A, 1981, vol. 43A, pp. 93–101.
H. Gleiter:Mater. Sci. Eng., 1982, vol. 52, pp. 91–131.
R.J. Pond and D. A. Smith:Phil. Mag., 1977, vol. 36, pp. 353–66.
D. Wolf:J. Phvsique, 1985, vol. 46 (Suppl. to No. 4), pp. C4 197–211.
R. W. Balluffi, Y. Komem, and T. Schober:Surf. Sci., 1972, vol. 31, pp. 68–103.
V. T. Borisov, V. M. Golikov, and G. V. Scherbedinskiy:Fiz. Met. Metaloved., 1964, vol. 17, pp. 881–85.
D. Gupta:Phil. Mag., 1976, vol. 33, pp. 189–97.
D. Gupta:Metall. Trans. A, 1977, vol. 8A, pp. 1431–38.
R. A. Perkins, R. A. Padgett, and N. K. Tunali:Metall. Trans., 1973, vol. 4, pp. 2535–40.
A. F. Smith and G. B. Gibbs:Met. Sci. J., 1969, vol. 3, pp. 93–94.
B. Weiss and R. Stickler:Metall. Trans., 1972, vol. 3, pp. 851–78.
L. E. Murr:Electron and Ion Microscopy and Microanalysis, Marcel Dekker Inc., New York and Basel, 1982, p. 740.
H.M. Ledbetter:Phys. Stat. Sol. (a), 1984, vol. 35, pp. 89–93.
T.P. Darby, R. Schindler, and R.W. Balluffi:Phil. Mag. A, 1978, vol. 37A, pp. 245–56.
P. H. Pumphrey:Phys. Stat. Sol. (a), 1975, vol. 28, pp. 545–53.
V. Linnenbom, M. Tetenbaum, and C. Cheek:J. Appl. Phys., 1955, vol. 26, pp. 32–35.
W. Assassa and P. Guiraldenq:Met. Sci., 1978, vol. 12, pp. 123–28.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Varin, R.A., Romanowska-Haftek, E. On the kinetics of the spreading of extrinsic grain boundary dislocations. Metall Trans A 17, 1967–1975 (1986). https://doi.org/10.1007/BF02644994
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02644994