Abstract
Both scanning transmission electron microscopic (STEM) and chemical extraction techniques were used to analyze the chemical content of precipitated austenite in 5.5Ni steel as a function of heat treatment. Austenite was introduced into the steel by tempering at 600 °C for 2 h (QT2) or 100 h (QT100), by tempering for 1 h at 670 °C (QL), or by double tempering 1 h at 670 °C + 1 h at 600 °C (QLT). The two methods of chemical analysis employed for the analysis of this austenite differ quantitatively in the measured austenite composition but are in qualitative agreement; they show an austenite enrichment in Ni, Cr, Mn, and Mo which is most pronounced (and nearly equivalent) for the QT100 and QLT treatments. The similar enrichment of the QT100 and QLT material is interpreted in light of the sequence of reactions leading to the QLT structure. A good correlation is found between the apparent solute enrichment of the precipitated austenite and its thermal stability on cooling to 77 K.
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Faculty Senior Scientist, Molecular & Materials Research Division, Lawrence Berkeley Laboratory, Berkeley, CA 94720.
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Kim, J.I., Morris, J.W. The composition of precipitated austenite in 5.5ni steel. Metall Trans A 12, 1957–1963 (1981). https://doi.org/10.1007/BF02643809
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DOI: https://doi.org/10.1007/BF02643809