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On the effect of stress on nucleation and growth of precipitates in an Al-Cu-Mg-Ag alloy

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Abstract

A study has been made of the effect of an externally applied tensile stress on Ω and Θ′ precipitate nucleation and growth in an Al-Cu-Mg-Ag alloy and a binary Al-Cu alloy which was used as a model system. Both solutionized and solutionized and aged conditions were studied. The mechanical properties have been measured and the microstructures have been characterized by transmission electron microscopy (TEM). The volume fraction and number density, as well as the precipitate size, have been experimentally determined. It was found that for as-solutionized samples aged under stress, precipitation occurs preferentially parallel to the stress axis. A threshold stress has to be exceeded before this effect can be observed. The critical stress for influencing the precipitate habit plane is between 120 and 140 MPa for Ω and between 16 and 19 MPa for Θ′ for the aging temperature of 160 °C. The major effect of the applied stress is on the nucleation process. The results are discussed in terms of the role of the lattice misfit between the matrix and the precipitate nucleus.

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References

  1. I.J. Polmear and M.J. Couper:Metall. Trans. A, 1988, vol. 19A, pp. 1027–35.

    CAS  Google Scholar 

  2. NASA Contractor Report No. 4645, Grant No. NAG-1-745, E.A. Starke, Jr., ed., NASA, Washington, DC, Feb. 1995.

  3. J.H. Auld:Acta Cryst., 1972, vol. A28, p. 98S.

  4. J.H. Auld:Mater. Sci. Technol., 1986, vol. 2, pp. 784–87.

    CAS  Google Scholar 

  5. S. Kerry and V.D. Scott:Met. Sci., 1984, vol. 18, pp. 289–94.

    Article  CAS  Google Scholar 

  6. K.M. Knowles and W.M. Stobbs:Acta Cryst., 1988, vol. B44, pp. 207–27.

    CAS  Google Scholar 

  7. B.C. Muddle and I.J. Polmear:Acta Metall., 1989, vol. 37, pp. 777–89.

    Article  CAS  Google Scholar 

  8. A. Garg and J.M. Howe:Acta Metall. Mater., 1991, vol. 39, pp. 1939–46.

    Article  CAS  Google Scholar 

  9. Y.C. Chang and J.M. Howe:Metall. Trans. A, 1993, vol. 24A, pp. 1461–70.

    CAS  Google Scholar 

  10. K. Hono, N. Sano, S.S. Babu, R. Okano, and T. Sakurai:Acta Metall. Mater., 1993, vol. 41, pp. 829–38.

    Article  CAS  Google Scholar 

  11. B.A. Shollock, C.R.M. Grovenor, and K.M. Knowles:Scripta Metall. Mater., 1990, vol. 24, pp. 1239–44.

    Article  CAS  Google Scholar 

  12. J.M. Howe:Phil. Mag. Lett., 1994, vol. 70, pp. 111–20.

    CAS  Google Scholar 

  13. K. Hono, T. Sakurai, and I.J. Polmear:Scripta Metall. Mater., 1994, vol. 30, pp. 659–700.

    Article  Google Scholar 

  14. W.F. Hosford and R.H. Zeisloft:Metall. Trans., 1972, vol. 3, pp. 113–21.

    CAS  Google Scholar 

  15. P. Bate, W.T. Roberts, and D.V. Wilson:Acta Metall., 1981, vol. 29, pp. 1797–1814.

    Article  CAS  Google Scholar 

  16. P. Bate, W.T. Roberts, and D.V. Wilson:Acta Metall., 1982, vol. 30, pp. 725–38.

    Article  CAS  Google Scholar 

  17. W.C. Johnson and C.S. Chiang:J. Appl. Phys., 1988, vol. 64, pp. 1155–65.

    Article  Google Scholar 

  18. C.S. Chiang and W.C. Johnson:J. Mater. Res., 1989, vol. 4, pp. 678–87.

    CAS  Google Scholar 

  19. M.R. Louthan, Jr.:Trans. AIME, 1963, vol. 227, pp. 1166–70.

    CAS  Google Scholar 

  20. M.R. Louthan, Jr. and C.L. Angeman:Trans. AIME, 1966, vol. 236, pp. 221–22.

    CAS  Google Scholar 

  21. Y. Nakada, W.C. Leslie, and T.P. Churay:Trans. ASM, 1967, vol. 60, pp. 223–27.

    CAS  Google Scholar 

  22. J.M. Oblak, D.F. Paulonis, and D.S. Duvall:Metall. Trans., 1974, vol. 5, pp. 143–53.

    CAS  Google Scholar 

  23. G. Sauthoff:Z. Metallkd., 1977, vol. 68, pp. 500–05.

    CAS  Google Scholar 

  24. W.F. Hosford and S.P. Agrawal:Metall. Trans. A, 1975, vol. 6A, pp. 487–91.

    CAS  Google Scholar 

  25. T. Eto, A. Sato, and T. Mori:Acta Metall., 1978, vol. 26, pp. 499–508.

    Article  CAS  Google Scholar 

  26. J.K. Tien and S.M. Copley:Metall. Trans., 1971, vol. 2, pp. 215–19.

    CAS  Google Scholar 

  27. T. Miyazaki, K. Nakamura, and H. Mori:J. Mater. Sci., 1979, vol. 14, pp. 1827–37.

    Article  CAS  Google Scholar 

  28. G. Lorimer:Precipitation Processes in Solids, K.C. Russel and I. Aaronson, eds., TMS-AIME, Warrendale, PA, 1978, pp. 87–160.

    Google Scholar 

  29. U.F. Kocks, J.S. Kallend, H.-R. Wenk, A.D. Rollett, and S.I. Wright:popLA—Preferred Orientation Package—Los Alamos, Los Alamos National Laboratory, Los Alamos, NM, July 1994.

  30. Annual Book of ASTM Standards, vol. 03.01,Metals—Mechanical Testing: Elevated and Low-Temperature Tests; Metallography, ASTM, Philadelphia, PA, 1992.

  31. E.E. Underwood:Quantitative Stereology, Addison-Wesley Publishing Company, Reading, MA, 1970, p. 178.

    Google Scholar 

  32. D.B. Williams:Practical Analytical Electron Microscopy in Materials Science, Verlag Chemie International, 1984, p. 78.

  33. J.C. Williams and E.A. Starke, Jr.: inDeformation, Processing and Structure, G. Krauss, ed., ASM, Metals Park, OH, 1984, pp. 279–354.

    Google Scholar 

  34. W.A. Cassada, G.J. Shiflet, and W.A. Jesser:Acta Metall. Mater., 1992, vol. 40, pp. 2101–11.

    Article  CAS  Google Scholar 

  35. E. Seitz and D. DeFontaine:Acta Metall., 1978, vol. 26, pp. 1671–79.

    Article  CAS  Google Scholar 

  36. U. Dahmer and K.H. Westmacott:Phys. Status Solidi A, 1983, vol. 80, pp. 249–62.

    Article  Google Scholar 

  37. S.P. Ringer, B.C. Muddle, and I.J. Polmear:Metall. Trans. A, 1995, vol. 26A, pp. 1659–71.

    CAS  Google Scholar 

  38. Z.M. Wang and G.J. Shiflet:Metall. Trans. A, 1996, vol. 27A, pp. 0000–00.

    Google Scholar 

  39. W.M. Stobbs and G.R. Purdy:Acta Metall., 1978, vol. 26, pp. 1069–81.

    Article  CAS  Google Scholar 

  40. G. Sauthoff:Z. Metallkd., 1975, vol. 66, pp. 106–09.

    CAS  Google Scholar 

  41. G. Sauthoff:Z. Metallkd., 1976, vol. 67, pp. 25–29.

    CAS  Google Scholar 

  42. R.W. Fonda, W.A. Cassada, and G.J. Shiflet:Acta Metall. Mater., 1992, vol. 40, pp. 2539–46.

    Article  CAS  Google Scholar 

  43. H.I. Aaronson, C. Laird, and K.R. Kinsman:Phase Transformation, ASM, Metals Park, OH, 1970, pp. 313–96.

    Google Scholar 

  44. B. Strotzki, H. Hargarter, and E.A. Starke, Jr.: inProc. 5th Int. Conf. on Aluminum Alloys, Their Physical and Mechanical Properties, Grenoble, France, July 1996, J.H. Driver, B. Dubost, F. Durand, R. Fourgers, P. Guyot, P. Sainfort, and M. Fuery, eds. pp. 1245–50, Materials Science Forum, vol. 217–222, 1966, Transtec Publications, Switzerland.

    Google Scholar 

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Skrotzki, B., Shiflet, G.J. & Starke, E.A. On the effect of stress on nucleation and growth of precipitates in an Al-Cu-Mg-Ag alloy. Metall Mater Trans A 27, 3431–3444 (1996). https://doi.org/10.1007/BF02595436

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