Skip to main content
Log in

Measurement of the size distribution of fat crystals using a laser particle counter

  • Technical
  • Published:
Journal of the American Oil Chemists’ Society

Abstract

A new method that uses a laser particle counter has been developed to measure the size of fat crystals. The fat crystals were suspended in isobutanol in the ratio of 1∶25,000. The solid and liquid fat recovery after being in contact with isobutanol for 24 hr, fatty acid composition of the solid and liquid fractions, DSC melting behavior and polarized light microscopy proved that isobutanol did not affect the structural integrity of the fat crystals. The mean crystal size of commercial shortenings ranged from 5 to 9 μm. The isobutanol suspension method makes it possible to quantitatively separate the solid and liquid components of a fat. It also provides a convenient way of preparing fat crystals for scanning electron microscopy.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Davis, S.S.,J. Texture Studies 4:15 (1973).

    Google Scholar 

  2. Ohlson, R., inDietary Fats and Health, AOCS Monograph No. 10., edited by E.G. Perkins and W.J. Visek, pp. 124–136 (1983).

  3. Bailey, A.E.,Melting and Solidification of Fats, Interscience Publishers, New York, NY, 1950.

    Google Scholar 

  4. deMan, J.M., and A.M. Beers,J. Texture Studies 18:303 (1987).

    Google Scholar 

  5. deJager, E.M., M. van den Tempel and P. deBruyne,Koninkl. Nederl. Akad. Wetenschap. Proc. Ser B. 66:17 (1963).

    CAS  Google Scholar 

  6. van Putte, K.P.A.M., and B.H. Bakker,J. Am. Oil Chem. Soc. 64:1138 (1987).

    Google Scholar 

  7. deMan, L., J.M. deMan and B. Blackman,66:128 (1989).

    Google Scholar 

  8. Poot, C., W. Dijkshoorn, A.J. Haighton and C.C. Verburg,52:69 (1975).

    CAS  Google Scholar 

  9. Albanese, F., inFat Science, Part A. Proc. 16th ISF Congr. Budapest, edited by J. Hollo, pp. 445–455 (1983).

Download references

Author information

Authors and Affiliations

Authors

About this article

Cite this article

Chawla, P., deMan, J.M. Measurement of the size distribution of fat crystals using a laser particle counter. J Am Oil Chem Soc 67, 329–332 (1990). https://doi.org/10.1007/BF02539684

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02539684

Keywords

Navigation