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Improving accuracy in routine instrumental activation analysis

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Abstract

An INAA procedure for routine analysis of rock samples is described. Samples are irradiated using a rotating sample holder. Measurement of the induced gamma activity is performed using an automatic gamma spectrometer and the elemental concentrations are calculated by a computer. The analytical error is discussed and the precision and accuracy evaluated experimentally. An average error of ±3–5% without considering counting statistics is obtained. Results for 19 elements in 8 international standard rocks are reported. A short discussion of the cost of the analysis is included.

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References

  1. R. J. ROSENBERG, Suomen Kemistilehti, 45B (1972) 399.

    Google Scholar 

  2. R. J. ROSENBERG, Proc. of the 7th Materials Research Symposium, Accuracy in Trace Analysis, NBS, Gaithesburg, October 7–11, 1974, NBS Spec. Publ. 422, Washington D. C., 1976, p. 1241.

  3. K. RUOTI, V. PITKÄNEN, P. Peltola, R. ROSENBERG, Reaktorilaboratorio, tiedonanto 35, VTT, Espoo, May 1976.

    Google Scholar 

  4. R. J. ROSENBERG, T. SEPPÄ-LASSILA, Reaktorilaboratorio, tiedonanto 15, VTT, Espoo, October 1972.

    Google Scholar 

  5. P. A. BAEDECKER, Proc. Symp. on Activation Analysis in Geochemistry and Cosmochemistry, A. O. BRUNFELT, E. STEINNES (Eds), Universitetsförlaget, Denmark, 1971, p. 145.

    Google Scholar 

  6. A. SAVITZKY, M. J. F. GOLAY, Anal. Chem., 36 (1964) 1627.

    Article  CAS  Google Scholar 

  7. F. J. FLANAGAN, Geochim. Cosmochim. Acta, 37 (1973) 1189.

    Article  CAS  Google Scholar 

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Rosenberg, R.J., Zilliacus, R. Improving accuracy in routine instrumental activation analysis. J. Radioanal. Chem. 39, 189–200 (1977). https://doi.org/10.1007/BF02517226

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  • DOI: https://doi.org/10.1007/BF02517226

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