Skip to main content
SpringerLink
Log in

Preliminary study of quality control of99mTc from99Mo generators

  • Analytical Control of Radiopharmaceuticals Section
  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

The separation of Tc(VII) from Mo(VI) by thin-layer and paper-chromatography is discussed. Some aspects concerning the formation and identification of lower oxidation states of Tc(VII) are also mentioned. Finally, a spot test is recommended for the determination of Mo(VI) and Al, which can be contaminants in the Tc(VII) solution eluted from the99Mo column, filled with Al2O3.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. K. E. Scheer, W. Maier-Borst,Nucl. Med., 3 (1963) 214.

    CAS  Google Scholar 

  2. Fr. 1.486.542 (Cl.G 21g, A61b) 30 June 1967 (CA, 68: 74.374n).

  3. E. Lieberman, W. J., Gemmil, U.S. 3.382.152 (Co.176-16), 7 May 1968 (CA,69 P 23842q).

  4. M. E. Garhy, S. El Bayoumy, S. El Alfy, Radiochem. Conf. Abstr. Pap., Bratislava, 1966, p. 27.

  5. A. Kulesza,Nukleonika, 14 (1969) 261.

    CAS  Google Scholar 

  6. P. Richards, Proc. Symp. on Recent Advances in Nuclear Medicine, Hahneman Medical College, 1967; USAEC Report BNL 9032, Brookhaven National Laboratory, 1964.

  7. V. Ravnik, R. Gorenc, J. Novak,Atompraxis, 13 (1967) 258.

    CAS  Google Scholar 

  8. C. Wen-Pin, Y. Si Yung,J. Chin. Chem. Soc. (Taipei), 15 (1968) 17.

    Google Scholar 

  9. S. Bulbulian, H. Sorantin,Kerntechnik, 8 (1966) 118.

    CAS  Google Scholar 

  10. L. Lindner, H. H. Stamm, Ger. 1.278.419 (Cl. C Olg), 26 Sept. 1968 (CA, 69, P 112.514b).

  11. S. Meloni, A. Brandone,Intern. J. Appl. Radiation Isotopes, 19 (1968) 164.

    Article  CAS  Google Scholar 

  12. M. El Garhy, Z. Moustafa, N. B. Mikheev,Atompraxis, 12 (1966) 93.

    Google Scholar 

  13. P. Richards, Proc. of Symp. at ORNL Radioactive Pharmaceuticals, USAEC, 1966, p. 323.

  14. E. P. Belkas, D. C. Perricos,Radiochim. Acta, 11 (1969) 56.

    CAS  Google Scholar 

  15. P. V. Harper, Medical Radioisotopes Scanning, Vol. II, IAEA, 1964, p. 36.

    Google Scholar 

  16. J. B. Gerlit, Proc. Intern. Conf. on the Peaceful Uses of Atomic Energy, United Nations, Vol. 7, 1956, p. 147.

    Google Scholar 

  17. M. S. Fadeev,Zh. Neorg. Khim., 3 (1958) 165.

    Google Scholar 

  18. G. E. Boyd, Q. V. Larson,J. Phys. Chem., 64 (1960) 988.

    CAS  Google Scholar 

  19. J. J. Pinajian, USAEC Report, ORNL-TM-1058, Oak Ridge National Lab., 1965.

  20. M. Anwar, K. Lathrop, D. Rosskelly, P. V. Harper,J. Nucl. Med., 9 (1968) 298.

    Google Scholar 

  21. C. Archundia, F. D. S. Butement,Rev. Soc. Quim. Mex., 12 (1968) 99A.

    CAS  Google Scholar 

  22. F. Krasovec, C. Klofutar, Proc. Intern. Conf. Solvent Extraction Chemistry, Göteborg, 1966.

  23. K. A. Gavrilov, J. Mikulski, T. S. Wang,Radiokhimiya, 10 (1968) 350.

    CAS  Google Scholar 

  24. R. Shanker, K. S. Venkateswarla, J. Shankar,J. Less-Common Metals, 15 (1968) 311.

    Article  CAS  Google Scholar 

  25. R. Richards,Intern. J. Appl. Radiation Isotopes, 17 (1966) 427.

    Article  CAS  Google Scholar 

  26. Y. Maki, K. Tanaka, K. K. Kogyo,Shikensho Kenkyo Hokoku, 20 (1968) 41.

    Google Scholar 

  27. H. Seiler,Helv. Chim. Acta, 52 (1969) 319.

    Article  CAS  Google Scholar 

  28. R. D. Peacock, R. Colton,Quart. Rev., 16 (1962) 299.

    Article  Google Scholar 

  29. S. K. Shukla,J. Chromatog., 21 (1966) 92.

    Article  CAS  Google Scholar 

  30. M. J. Williams, T. Deegan,J. Chromatog., 54 (1971) 123.

    Article  CAS  Google Scholar 

  31. R. Muenze,Z. Phys. Chem., 238 (1968) 364.

    CAS  Google Scholar 

  32. R. Colton, J. Dalziel, W. P. Griffith, G. Wilkinson,J. Chem. Soc., (1960) 71.

  33. L. B. Rogers,J. Am. Chem. Soc., 71 (1949) 1507.

    CAS  Google Scholar 

  34. R. J. Magee, I. A. P. Scot, C. L. Wilson,Talanta, 2 (1959) 376.

    Article  CAS  Google Scholar 

  35. R. Colton, J. A. W. Dalziel, W. P. Griffith, G. Wilkinson,Nature, 183 (1959) 1755.

    Article  CAS  Google Scholar 

  36. H. H. Miller, M. T. Kelley, P. F. Thomason,Adv. Polarogr., 2 (1960) 716.

    Google Scholar 

  37. D. L. Love, A. E. Greendale,Anal. Chem., 32 (1960) 780.

    Article  CAS  Google Scholar 

  38. A. F. Kuzina, S. I. Zhdanov, V. J. Spitsyn,Dokl. Akad. Nauk. SSSR, 144 (1962) 836.

    CAS  Google Scholar 

  39. A. A. Terry, H. F. Zittel,Anal. Chem., 35 (1963) 614.

    Article  CAS  Google Scholar 

  40. G. B. S. Salaria, C. L. Rulfs, P. J. Elving,J. Chem. Soc., (1963) 2479.

  41. G. B. S. Salaria, C. L. Rulfs, P. J. Elving,Anal. Chem., 35 (1963) 979.

    Article  CAS  Google Scholar 

  42. G. B. S. Salaria, C. L. Rulfs, P. J. Elving,Anal. Chem., 36 (1964) 146.

    Article  CAS  Google Scholar 

  43. R. Münze,Z. Phys. Chem., 226 (1964) 415.

    Google Scholar 

  44. C. L. Rulfs, R. Pacer, A. Anderson,J. Electroanal. Chem., 15 (1967) 61.

    Article  CAS  Google Scholar 

  45. C. L. Rulfs, R. Pacer, R. Hirsch,J. Inorg. Nucl. Chem., 29 (1967) 681.

    Article  CAS  Google Scholar 

  46. L. Astheimer, K. Schwochau,J. Electroanal. Chem., 14 (1967) 240.

    Article  CAS  Google Scholar 

  47. L. Astheimer, K. Schwochau, W. Herr,J. Electroanal. Chem., 14 (1967) 161.

    Article  CAS  Google Scholar 

  48. S. A. Zhdanov, A. F. Kuzina, V. I. Spitsyn,Zh. Neorg. Khim., (1970) 1567.

  49. R. E. Voltz, M. L. Holt,J. Electrochem. Soc., 114 (1967) 128.

    CAS  Google Scholar 

  50. G. Kissel, S. W. Feldberg,J. Phys. Chem., 73 (1969) 3082.

    Article  CAS  Google Scholar 

  51. K. V. Kotegov, O. N. Pavlov, V. P. Shvedov,Adv. Inorg. Chem. Radiochem., 11 (1968) 2.

    Google Scholar 

  52. P. Vesely, J. Cifka, Some chemical and analytical problems connected with99mTc generator, IAEA Panel on Preparation and Control of Radiopharmaceuticals from Generators-produced Radioisotope in Medical Laboratories, Vienna, 11–15 May, 1970.

  53. B. L. Clarke, H. W. Hermance,Ind. Eng. Chem. Anal. Ed., 9 (1963) 292. (From Spot Tests in Inorganic Analysis byF. Feigl, Elsevier, Amsterdam-London-New York-Princeton, 1958, p. 116.)

    Article  Google Scholar 

  54. F. L. Hahn,Mikrochemie, 11 (1932) 33. (From Spot Tests in Inorganic Analysis byF. Feigl, Elsevier, Amsterdam-London-New York-Princeton, 1958, p. 116.)

    Google Scholar 

  55. G. Charlot, Les Méthodes de la Chimie Analytique, Masson, Paris 1961, p. 589.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. International Atomic Energy Agency Laboratory, Seibersdorf, Vienna, (Austria)

    L. Oniciu & G. B. Cook

Authors
  1. L. Oniciu
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. G. B. Cook
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Oniciu, L., Cook, G.B. Preliminary study of quality control of99mTc from99Mo generators. J. Radioanal. Chem. 13, 247–254 (1973). https://doi.org/10.1007/BF02514128

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02514128

Keywords

Search

Navigation