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The preparation of high-purity magnesium oxide

I. Separation of microquantities of calcium from macroquantities of magnesium

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Abstract

The results are presented of an investigation with the radioactive isotope45Ca of processes of coprecipitation, crystallization and liquid—liquid extraction of calcium for the preparation of high-purity salts of magnesium.

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References

  1. F. W. E. Strelow, C. R. Van Zyl,Anal. Chim. Acta, 41 (1968) 529.

    Article  CAS  Google Scholar 

  2. Z. Winowski,Chem. Anal. (Warsaw), 12 (1967) 1271.

    CAS  Google Scholar 

  3. F. J. Welcher, The Analytical Uses of Ethylenediaminetetraacetic Acid, Van Nostrand Co., New York, 1958.

    Google Scholar 

  4. J. A. Tarkovskaya, F. P. Gorbenko,Zh. Analit. Khim., 20 (1965) 1185.

    CAS  Google Scholar 

  5. G. A. Bornemann, W. F. McIlhenny, U. S. Patent 3,341,290, 1967.

  6. L. Ya. Polyak,Zavodsk. Lab., 27 (1961) 803.

    CAS  Google Scholar 

  7. P. Povondra, R. Pribil,Talanta, 10 (1963) 713.

    Article  CAS  Google Scholar 

  8. D. Yoshiko, T. Kyoji,Bull. Chem. Soc. Japan, 36 (1963) 518.

    Article  Google Scholar 

  9. M. Milan,Anal. Chem., 42 (1970) 652.

    Article  Google Scholar 

  10. I. I. Angelov, G. A. Pevtsov, M. M. Shvarts,Trudy Vsesoyuz. Nauch-Issledovatel. Inst. Khim. Reaktivov, 23 (1959) 31.

    Google Scholar 

  11. S. N. Poddar, N. R. Sengupta,Indian J. Chem., 1 (1963) 495.

    CAS  Google Scholar 

  12. D. P. Joshi, D. V. Jain,J. Indian Chem. Soc., 41 (1964) 711.

    CAS  Google Scholar 

  13. P. L. Robinson, W. E. Scott,Z. Anal. Chem., 88 (1932) 417.

    Article  CAS  Google Scholar 

  14. R. Fresenius, G. Jander, Handbuch der analytischen Chemie, Vol. II, Berlin, 1955.

  15. D. C. Nonova,Mikrochim. Acta, (1958) 111.

  16. C. C. Washbrook,Analyst, 75 (1950) 621.

    Article  CAS  Google Scholar 

  17. H. Imai,Chem. Abstr., 52 (1958) 7020 c.

  18. Z. Marczenko, Organic Reagents in Inorganic Analysis, PWN, Warsaw, 1959, p. 503 (in Polish).

    Google Scholar 

  19. N. T. Sizonenko, E. S. Zolotovitskaya,Zh. Analit. Khim., 21 (1966) 264.

    CAS  Google Scholar 

  20. J. W. Mellor, Inorganic and Theoretical Chemistry, London, 1963.

  21. Spravochnik Khimiya, Moscow, 1951, Vol. I.

  22. A. P. D. Seidell, Solubilities of Inorganic and Metal Organic Compounds, New York, 1940.

  23. F. Umland, K. U. Meckenstock,Z. Anal. Chem., 96 (1960) 176.

    Google Scholar 

  24. F. P. Gorbenko, V. V. Sachko,Zh. Analit. Khim., 20 (1965) 1198.

    Google Scholar 

  25. Yu. A. Zolotov, V. G. Lambrev,Zh. Analit. Khim., 20 (1965) 659.

    CAS  Google Scholar 

  26. A. K. De, S. M. Khopkar, R. A. Chalmers, Solvent Extraction of Metals, Van Nostrand Reinhold Co., London 1971, p. 259.

    Google Scholar 

  27. A. K. De, S. M. Khopkar,J. Sci. Ind. Res. (India), 21A (1962) 131.

    Google Scholar 

  28. T. Sekine, D. Dyrssen,Anal. Chim. Acta, 37 (1967) 217.

    Article  CAS  Google Scholar 

  29. R. B. Quincy, Jr., ORNL-TM-302, 1962.

  30. M. H. Leipold, T. H. Nielsen,Am. Ceram. Soc. Bull., 45 (1966) 281.

    CAS  Google Scholar 

  31. J. Akaza,Bull. Chem. Soc. Japan, 39 (1966) 971.

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Institute of Inorganic Chemistry and Technology, Technical University, Gliwice, (Poland)

    A. Dębska-Horecka & T. Pukas

  2. Laboratory of Chemistry and Radiochemistry, Institute of Nuclear Physics, Kraków-Bronowice, (Poland)

    I. Stroński

Authors
  1. A. Dębska-Horecka
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  2. T. Pukas
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  3. I. Stroński
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Dębska-Horecka, A., Pukas, T. & Stroński, I. The preparation of high-purity magnesium oxide. J. Radioanal. Chem. 13, 21–30 (1973). https://doi.org/10.1007/BF02514105

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  • DOI: https://doi.org/10.1007/BF02514105

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