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Headspace solid-phase microextraction and gas chromatography-mass spectrometry analysis of free volatile compounds inMango

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Summary

Manual headspace—solid-phase microextraction (HS-SPME) gas chromatography-mass spectrometry (GC-MS), a simple, rapid and sensitive method, was employed for the identification and quantitative analysis of the main volatile constituents inMango juice. Nineteen compounds were quantified though standard addition. The main volatile compounds ofMango juice were terpenes, including mono-or sesquiterpene hydrocarbons, such as 1R-α-pinene, 3-carene, α-terpinene, limonene, E-α-ocimene, terpinolene, eremophiladiene, α-caryophyllene, and guaiadiene with concentrations varying from 4 to 8000 μg L−1. The factors affecting quantitative results, including absorption time, speed of stirring and ionic strength are discussed.

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Authors and Affiliations

  1. Center for Analysis & Measurement, Fudan University, 200433, Shanghai, P.R. China

    Chunqing Shang & Yaoming Hu

  2. Department of Chemistry, Fudan University, 200433, Shanghai, P.R. China

    Chunhui Deng & Xiaoyue Zhang

  3. State Key Laboratory of Pollution Control and Resources Reuse, Tongji University, 200092, Shanghai, P.R. China

    Zhengfu Chen

Authors
  1. Chunqing Shang
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  2. Chunhui Deng
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  3. Xiaoyue Zhang
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  4. Zhengfu Chen
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  5. Yaoming Hu
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Shang, C., Deng, C., Zhang, X. et al. Headspace solid-phase microextraction and gas chromatography-mass spectrometry analysis of free volatile compounds inMango . Chromatographia 55, 737–741 (2002). https://doi.org/10.1007/BF02491790

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  • DOI: https://doi.org/10.1007/BF02491790

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